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Titanium electrorefining process, carried out in cell with anode formed by molten titanium mixture, solid titanium cathode and electrolyte comprising molten salt and titanium dichloride

机译:钛电精炼工艺,在电解槽中进行,阳极由熔融钛混合物,固体钛阴极和含熔盐和二氯化钛的电解质组成

摘要

Titanium is dissolved in a metal which is more inert and this mixture is melted to forming the anode. Electrolysis is then carried out using an electrolyte comprising a molten salt mixture and titanium dichloride, and a solid titanium cathode. A process for electrorefining titanium from a metal mixture in an electrolysis cell comprises the following steps: (A) dissolving the titanium in at least one different metal which is more inert than titanium; (B) forming an anode by melting the titanium-containing mixture; (C) using an electrolyte comprising a molten salt mixture and titanium dichloride; and (D) using a cathode comprising solid titanium. Independent claims are also included for the following: (1) method for preparing a metal mixture comprising titanium and at least one other metal which is more inert than titanium, by preparing a solution of titanium in the metal by adding rutile, titania or titanium tetrachloride to an electrolysis cell containing a graphite anode, an electrolyte comprising a liquid calcium chloride mixture, and a cathode formed by one or more liquid metals which are more inert than titanium; and (2) apparatus for carrying out the first method.
机译:钛溶解在惰性更高的金属中,该混合物熔化形成阳极。然后使用包含熔融盐混合物和二氯化钛的电解质以及固体钛阴极进行电解。从电解池中的金属混合物中电提纯钛的方法包括以下步骤:(A)将钛溶解在至少一种比钛惰性的不同金属中; (B)通过熔融含钛混合物形成阳极; (C)使用包含熔融盐混合物和二氯化钛的电解质; (D)使用包含固体钛的阴极。还包括以下方面的独立权利要求:(1)通过加入金红石,二氧化钛或四氯化钛制备钛在金属中的溶液,从而制备包含钛和至少一种比钛更惰性的其他金属的金属混合物的方法。电解槽包括石墨阳极,包含液态氯化钙混合物的电解质和由一种或多种比钛惰性的液态金属形成的阴极; (2)用于执行第一方法的设备。

著录项

  • 公开/公告号NL1030349C2

    专利类型

  • 公开/公告日2007-05-07

    原文格式PDF

  • 申请/专利权人 ANTHONIE VAN SANDWIJK;

    申请/专利号NL20051030349

  • 发明设计人 ANTHONIE VAN SANDWIJK;

    申请日2005-11-04

  • 分类号C25C3/28;

  • 国家 NL

  • 入库时间 2022-08-21 20:57:05

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