首页> 外国专利> Zero headspace extractor and method for determining partitioning and contaminant release rates of volatile and semi-volatile compounds

Zero headspace extractor and method for determining partitioning and contaminant release rates of volatile and semi-volatile compounds

机译:零顶空萃取器和确定挥发性和半挥发性化合物的分配和污染物释放速率的方法

摘要

A method and device for measuring release rates of contaminants in at least one of a fast release mode and a slow release mode in which a volatile liquid sample is introduced into a sealed transparent reactor vessel having at least one sorbent contained within the transparent reactor vessel and a separator for preventing direct contact between the at least one adsorbent and the at least one volatile liquid sample in the transparent reactor vessel, whereby substantially zero headspace is maintained within the transparent reactor vessel. At least one solvent soluble constituent present in the at least one volatile liquid sample is passed through the separator, resulting in sorption of the at least one solvent soluble constituent by the at least one sorbent. In accordance with one preferred embodiment, the separator is a dialysis bag contained in the transparent reactor vessel into which the resin is placed. The at least one solvent soluble constituent is then removed from the at least one sorbent through the separator.
机译:一种用于在快速释放模式和缓慢释放模式中的至少一种模式下测量污染物释放速率的方法和装置,在该模式和装置中,将挥发性液体样品引入到密封的透明反应器容器中,该密封的透明反应器容器中至少含有一种吸附剂,并且隔离器,用于防止透明反应器容器中的至少一种吸附剂和至少一种挥发性液体样品之间的直接接触,从而在透明反应器容器内保持基本上零的顶空。使存在于至少一种挥发性液体样品中的至少一种溶剂可溶成分通过分离器,从而导致至少一种吸附剂吸附至少一种溶剂可溶成分。根据一个优选的实施方案,分离器是容纳在透明反应容器中的透析袋,树脂被放置在该透明反应容器中。然后通过分离器从至少一种吸附剂中除去至少一种溶剂可溶成分。

著录项

  • 公开/公告号US7189579B2

    专利类型

  • 公开/公告日2007-03-13

    原文格式PDF

  • 申请/专利权人 BHUPENDRA K. SONI;THOMAS D. HAYES;

    申请/专利号US20020080475

  • 发明设计人 BHUPENDRA K. SONI;THOMAS D. HAYES;

    申请日2002-02-22

  • 分类号G01N1/18;G01N1/00;G01N1/22;G01N1/10;B32B5/02;

  • 国家 US

  • 入库时间 2022-08-21 21:01:49

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