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首页> 外国专利> 1,2,3-TRIS-{AMINOPOLY(ETHYLENEAMINO)ETHYLAMMONIO-METHYLCARBONYLOXYPOLY(ALKYLENEOXY)}PROPANE TRICHLORIDES POSSESSING FUNGICIDE ACTIVITY, PROPERTY OF EMULSIFIER OF CATIONIC BITUMEN EMULSION, CAPACITY TO ENHANCE ADHESION OF BITUMEN TO MINERAL MATERIALS AND METHOD FOR THEIR PREPARING

1,2,3-TRIS-{AMINOPOLY(ETHYLENEAMINO)ETHYLAMMONIO-METHYLCARBONYLOXYPOLY(ALKYLENEOXY)}PROPANE TRICHLORIDES POSSESSING FUNGICIDE ACTIVITY, PROPERTY OF EMULSIFIER OF CATIONIC BITUMEN EMULSION, CAPACITY TO ENHANCE ADHESION OF BITUMEN TO MINERAL MATERIALS AND METHOD FOR THEIR PREPARING

机译：1,2,3-TRIS-{[酰胺基（乙酰胺基）乙基铵]-甲基碳氧羰基（烷基乙氧基）]}丙三醇具有杀真菌剂的活性，阳离子型乳化剂的乳化剂的性质，对方法的抵抗力和增强的能力准备中

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FIELD: organic chemistry, chemical technology.;SUBSTANCE: invention relates to novel 1,2,3-tris-{[aminopoly(ethyleneamino)ethylammonio]-methylcarbonyloxypoly(alkyleneoxy)]}propane trichlorides of the formula:; wherein at a + c + e (the general degree of oxypropylation) = 49; b + d + f (the general degree of ethylation) = 0, n = 1-6; at a + c + e = 55, b + d + f = 0, n = 1-6; at a + c + e = 49, b + d + f = 9, n = 1-6; at a + c + e = 10, b + d + f = 10, n = 1-6; at a + c + e = 66, b + d + f = 15, n = 1-6; at a + c + e = 76, b + d + f = 18, n = 1-6, and to a method for their synthesis. Method involves interaction of 1,2,3-tris-[hydroxypoly(alkyleneoxy)]propanes of the formula:; wherein a + c + e = 49-76, b + d + f = 0-18 with monochloroacetic acid in the presence of acidic catalysts, in boiling organic solvent medium, azeotropic removing water formed and the following treatment at heating the synthesized reaction product with polyethylenepolyamines of the formula: H2N(CH2CH2NH)nCH2CH2NH2 wherein n = 1-6, and in the following mole ratios of reagents - hydroxyl derivatives of propane : monochloroacetic acid : polyethylenepolyamines = 1:(3.0-3.2):(3.0-3.2), respectively. New compounds possess the fungicide activity, properties of emulsifiers of cationic bitumen emulsions, capacity to enhance adhesion of bitumen to mineral materials.;EFFECT: improved preparing method, valuable properties of compounds.;6 cl, 3 tbl, 6 ex
机译：发明领域：本发明涉及新型的1,2,3-三-{[氨基聚（乙烯氨基）乙基铵]-甲基羰基氧基聚（亚烷基氧基）]}丙烷三氯化物： 其中a + c + e（羟丙基化的一般程度） = 49; b + d + f（一般的乙基化度）= 0，n = 1-6;在a + c + e = 55时，b + d + f = 0，n = 1-6;在a + c + e = 49时，b + d + f = 9，n = 1-6;在a + c + e = 10时，b + d + f = 10，n = 1-6;在a + c + e = 66时，b + d + f = 15，n = 1-6;在a + c + e = 76，b + d + f = 18，n = 1-6的情况下，求出它们的合成方法。该方法涉及下式的1,2,3-三-[羟基聚（亚烷氧基）]丙烷的相互作用： 其中a + c + e = 49-76，b + d在酸性催化剂的存在下，在沸腾的有机溶剂介质中，用一氯乙酸+ f = 0-18，共沸除去形成的水，并在将合成的反应产物与下式的聚乙烯<！ > N（CH 2 CH 2 NH） n CH 2 CH 2 NH 2 其中n ＝ 1-6，并且在以下试剂的摩尔比下：丙烷的羟基衍生物：一氯乙酸：聚乙烯多胺＝ 1：（3.0-3.2）：( 3.0-3.2）。新化合物具有杀菌活性，阳离子沥青乳化剂的乳化剂性能，增强沥青与矿物材料的附着力的作用;效果：改进的制备方法，化合物的有价值的性能; 6 cl，3 tbl，6 ex

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