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SPECIMEN PRETREATING DEVICE AND PROBE USED THEREFOR

机译:标本预处理设备并探究其用途

摘要

[PROBLEMS] To prevent a specimen from being diffused by the improper capacity of tubing. [MEANS FOR SOLVING PROBLEMS] This specimen pretreating device comprises a micro scale or nano scale high-speed liquid chromatograph having a capillary column (2), a probe (1) integrally formed at the tip of the capillary column (2), and an additive feeding flow passage (16). The probe (1) is formed in a multi-tube structure in which a plurality of tubes are disposed on a same axis. The innermost tube is located at the tip of the capillary column (2), and one of the outer tubes is used as an additive supply tube converging an additive solution to an eluent solvent eluted from the capillary column (2) to form liquid drips including the eluent solvent and an additive and the liquid drips are dripped from the tip of the probe (1). The specimen is not diffused since a detector is not present in the flow passage.
机译:[问题]为了防止标本因管道容量不足而扩散。 [解决问题的手段]该样品前处理装置包括具有毛细管柱(2),在毛细管柱(2)的前端一体形成的探针(1)的微米级或纳米级高速液相色谱仪。添加剂进料流道(16)。探针(1)形成为多管结构,其中多个管布置在同一轴线上。最里面的管位于毛细管柱(2)的顶端,外部管之一用作添加剂供应管,它将添加剂溶液汇聚到从毛细管柱(2)洗脱的洗脱液中形成滴液,包括从探针(1)的尖端滴下洗脱液,溶剂和添加剂以及滴液。由于流道中不存在检测器,因此样本不会扩散。

著录项

  • 公开/公告号WO2006025367A1

    专利类型

  • 公开/公告日2006-03-09

    原文格式PDF

  • 申请/专利权人 SHIMADZU CORPORATION;IWATA YOSUKE;

    申请/专利号WO2005JP15734

  • 发明设计人 IWATA YOSUKE;

    申请日2005-08-30

  • 分类号G01N30/84;G01N27/62;G01N27/64;G01N30/72;G01N30/80;

  • 国家 WO

  • 入库时间 2022-08-21 21:32:06

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