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Temperature calibration method of thermal analysis equipment, temperature calibration equipment of thermal analysis equipment, and thermal analysis equipment
Temperature calibration method of thermal analysis equipment, temperature calibration equipment of thermal analysis equipment, and thermal analysis equipment
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机译:热分析设备的温度校准方法,热分析设备的温度校准设备和热分析设备
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摘要
PROBLEM TO BE SOLVED: To accurately calibrate the measuring result by a temperature measuring system used in a thermal analyzer for measuring items to be measured such as current, voltage, electric resistance, dielectric constant, electrostatic capacity, thermoelectromotive force, thermal stimulation current or the like related to a sample.;SOLUTION: This temperature calibrating method for the thermal analyzer is constituted so as to measure not only the temperature of a measuring sample set between electrode rods 6a and 6b in place of a reference substance 44 with a temperature sensor 34 but also the current, voltage, electric resistance or the like of the measuring sample while changing the temperature of the measuring sample. The temperature, at a time when the reference substance 44 is melted and a weight 46 cuts the reference substance 44 to fall, is actually measured as a melting temperature by the temperature sensor 34 and the temperature measured by the temperature sensor 34 is calibrated on the basis of a difference between the actually measured value and the literature value of the melting temperature of the reference substance 44.;COPYRIGHT: (C)2004,JPO&NCIPI
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