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The recovery equipment and method of copper sulfate from spent soft etching solution for recycling etching solution

机译:从废软蚀刻液中回收硫酸铜以回收蚀刻液的设备和方法

摘要

PURPOSE: A method and an apparatus for recovering molten copper sulfate for recycling waste soft etchant are provided to recycle waste etchant generated in various soft etching processes during fabrication of printing circuit boards by recovering copper sulfate molten in waste etchant and enabling the waste etchant to be reused. CONSTITUTION: The apparatus for recovering molten copper sulfate for recycling waste soft etchant comprises an evaporating and concentrating tank(30) connected to an etching tank(10) for performing soft etching of printing circuit boards to remove moisture and stench of the waste etchant flown in from the etching tank and evaporate and concentrate the waste etchant; first cooling tank(21) for first cooling the waste etchant flown in after being evaporated and concentrated in the evaporating and concentrating tank; second cooling tank(22) for second cooling the waste etchant flown in after being first cooled in the first cooling tank; a cooler(50) connected to the first and second cooling tanks through cooling line(51) to cool the waste etchant of the cooling tanks; a seed injection port(23) formed at one side of an upper part of the second cooling tank; a crystal recovery unit(24) connected to the center of a lower part of the second cooling tank to recover copper sulfate crystal precipitated; a recycling tank(40) connected to the second cooling tank so that the recycling tank injects the prepared etchant into the etching tank again after preparing an etchant by adding sulfuric acid, hydrogen peroxide and water to the waste etchant as much as the copper sulfate recovered after an etchant from which the copper sulfate crystal is recovered is flown into the recycling tank; and a line heater(70) formed on connection line of the etching tank and recycling tank to recover temperature of the cooled etchant again.
机译:目的:提供一种回收熔融硫酸铜以回收废软蚀刻剂的方法和设备,以通过回收废蚀刻剂中熔融的硫酸铜并使废蚀刻剂回收来回收印刷电路板制造过程中各种软蚀刻工艺中产生的废蚀刻剂。重用。构成:用于回收熔融硫酸铜以回收废软蚀刻剂的设备,包括与浓缩槽(10)相连的蒸发浓缩槽(30),该蚀刻槽用于对印刷电路板进行软蚀刻以去除流入的湿蚀刻剂的水分和臭味。从蚀刻槽中蒸发并浓缩废蚀刻剂。第一冷却槽(21),用于首先冷却在蒸发浓缩槽中蒸发浓缩后流入的蚀刻液。第二冷却槽(22),用于对在第一冷却槽中首先冷却后流入的蚀刻液进行第二冷却。冷却器(50)通过冷却管线(51)连接到第一和第二冷却槽,以冷却冷却槽的废蚀刻剂;在第二冷却槽的上部的一侧形成有种子注入口(23)。结晶回收单元(24),其连接于第二冷却槽下部的中央,回收析出的硫酸铜结晶。连接到第二冷却槽的再循环槽(40),以便在通过向废蚀刻剂中添加硫酸,过氧化氢和水至回收的硫酸铜的量制备蚀刻剂之后,再循环槽将制备好的蚀刻剂再次注入蚀刻槽中。从中回收了硫酸铜晶体的蚀刻剂流入回收罐后;在蚀刻槽和再循环槽的连接线上形成有线加热器(70),以再次恢复冷却的蚀刻剂的温度。

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