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Optical excitation inversion evaluation method of ferroelectric ceramics using acoustic emission technique

机译:基于声发射技术的铁电陶瓷光激发反演评估方法

摘要

The present invention relates to a method for evaluating the photoexcited region reversal of ferroelectric ceramics under light irradiation using an acoustic emission (AE) technique.;The present invention concentrates light having energy above the band gap from the xenon lamp 1 on the ferroelectric ceramic specimen 4 through the waveguide 2 and the lens 3 to form non-excited electrons trapped at the grain boundaries. As the division reversal occurs due to the space charge electric field, acoustic emission is caused by the release of temporary elastic energy, which is detected by the acoustic emission sensor 5, filtered through the band filter 7, and then amplified by the preamplifier 8. After analyzing in the AET 5500 system 10 connected to the computer 9, the acoustic excitation events with the peak height above the threshold voltage were counted for the light irradiation time, and then the occurrence rate of the photoexcitation region reversal activity was calculated. Can be evaluated qualitatively and the amount of change in light pressure current can be determined from a calibration curve between a predetermined sound emission event occurrence rate and the light pressure current change rate. It can be unpredictable.;Also, for the acoustic emission signals detected by the present invention, energy = peak height (dB) + 10 log (duration time (μs) is obtained and the energy is obtained. From the group, the acoustic emission signal due to the 180 ° and 90 ° region inversion of the ferroelectric ceramics having a tetragonal structure can be separated.
机译:本发明涉及一种利用声发射(AE)技术评估光照射下的铁电陶瓷的光激发区反转的方法。本发明将能量大于氙灯1的带隙的光聚集在铁电陶瓷样品上穿过波导2和透镜3的图4中所示的光形成形成在晶界处的非激发电子。当由于空间电荷电场而发生划分反转时,声发射是由于释放临时弹性能量而引起的,该临时弹性能量由声发射传感器5检测到,并通过带通滤波器7滤波,然后由前置放大器8放大。在连接至计算机9的AET 5500系统10中进行分析之后,将峰值高度高于阈值电压的声激发事件计数为光照射时间,然后计算光激发区域反转活性的发生率。可以定性地进行评估,并且可以从预定的声音发射事件发生率和气压电流变化率之间的校准曲线确定气压电流的变化量。另外,对于本发明检测到的声发射信号,能量=峰高(dB)+ 10log(持续时间(μs)),并且获得能量。具有四边形结构的铁电陶瓷由于180°和90°区域反转而产生的信号可以被分离。

著录项

  • 公开/公告号KR100302324B1

    专利类型

  • 公开/公告日2001-12-28

    原文格式PDF

  • 申请/专利权人 한국과학기술원;

    申请/专利号KR19980024379

  • 发明设计人 최시경;최동구;김성렬;

    申请日1998-06-26

  • 分类号G01N29/00;

  • 国家 KR

  • 入库时间 2022-08-22 00:31:58

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