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Glass transition temperature evaluation method for polymer material, involves calculating characteristic relaxation time of polymer material and setting relaxation chart during initial state of polymer material
Glass transition temperature evaluation method for polymer material, involves calculating characteristic relaxation time of polymer material and setting relaxation chart during initial state of polymer material
The proposed method allows to determine by dielectrometry the variation of the glass-transition temperature (Tg) of a polymer material used in the presence of fluids (water/organic compound/gas), pure or in admixture. More precisely, the invention is based on the use of dielectric sensors whose geometry is such that they allow to follow, in a sensitive and reproducible way, the frequency and/or temperature dependence of the dielectric permittivity characteristics of a polymer material in the presence of fluids without disturbing permeation/desorption of the solute during transient and unsteady states, these dielectric measurements (real and/or imaginary part) being connected with the plasticized state of the material, which determines the performances thereof during use.
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