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Preparation of 4,4'-dihydroxy-alpha'-dialkylstilbenes and 4, 4'- dihydroxy- alpha'-dialkylstilbenes
Preparation of 4,4'-dihydroxy-alpha'-dialkylstilbenes and 4, 4'- dihydroxy- alpha'-dialkylstilbenes
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机译：制备4,4'-二羟基-α'-二烷基芪和4,4'-二羟基-α'-二烷基芪
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摘要
4,4'-Dihydroxy-alpha-alkylstilbenes of high purity are prepared by reacting at a temperature of from about -20° C. to about 20° C. a mixture of (1) at least one alpha-haloketone, (2) at least one phenolic hydroxyl-containing compound or alkoxy-containing aromatic compound, and (3) at least one strong protonic acid or Lewis acid; such that the mole ratio of phenolic hydroxyl-containing compound or alkoxy- containing aromatic compound:alpha-haloketone(s) is from 0.1:1 to 1.9:1, and the mole ratio of phenolic hydroxyl-containing compound or alkoxy- containing aromatic compound:alpha-haloketone(s):strong protonic acid or Lewis acid is from about 0.1:1:0.0026 to about 1.9:1:0.95. The high purity 4,4'-dihydroxy-alpha-alkylstilbenes are useful for the advancement of epoxy resins, for the preparation of phenoxy resins and for the preparation of epoxy resins.
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