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Experimental vessel for high temperature graphite coated with silicon nitride film (Si_3N_4) or silicon oxide film (SiO_2) and its fabrication method

机译:氮化硅膜Si_3N_4或氧化硅膜SiO_2的高温石墨实验容器及其制造方法

摘要

The present invention relates to a graphite test vessel in which graphite is used as a material and a silicon nitride film or a silicon oxide film is coated thereon. The present invention also relates to a method of manufacturing a graphite sheet, comprising the steps of: a) machining a commercially available graphite into a desired shape, b) depositing the graphite in a chemical vapor deposition reactor in a chemical vapor deposition reactor, And c) when the coating operation is completed, the gas atmosphere is adjusted to nitrogen or oxygen depending on the type of the film, and then heat treatment is performed at 600-900C for about 1 hour to remove pinholes that may be present. . The graphite test vessel manufactured according to the present invention is excellent in radiant heat absorbing ability for maximizing the effect of rapid heating when a rapid heating type radiating furnace is used. It is also possible to coat a silicon nitride film or a silicon oxide film with a chemical vapor deposition And it is remarkably improved in terms of performance and price compared with the conventional platinum container and the like.
机译:石墨测试容器技术领域本发明涉及一种石墨测试容器,其中使用石墨作为材料并且在其上涂覆氮化硅膜或氧化硅膜。本发明还涉及一种制造石墨片的方法,其包括以下步骤:a)将可商购获得的石墨加工成期望的形状,b)将石墨沉积在化学气相沉积反应器中的化学气相沉积反应器中,以及c)当涂布操作完成时,根据膜的类型将气体气氛调节为氮气或氧气,然后在600-900℃下进行约1小时的热处理以除去可能存在的针孔。 。根据本发明制造的石墨测试容器具有优异的辐射吸热能力,以在使用快速加热型辐射炉时最大化快速加热的效果。还可以通过化学气相沉积来涂覆氮化硅膜或氧化硅膜,并且与常规的铂容器等相比,在性能和价格上得到显着改善。

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