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Low energy extractive distillation process for producing anhydrous ethanol

机译:低能萃取蒸馏法生产无水乙醇

摘要

A thermally-integrated extractive distillation process for recovering anhydrous ethanol from fermentation or synthetic feedstocks has a distillation train of four columns. Two columns are preconcentrators operated in parallel. The remaining columns are an extractive distillation dehydrating tower, and an entrainer-recovery column. The two preconcentrators and the dehydrating tower are operated at three successively increasing pressures so that the condensing vapors of the overhead product of the dehydrating tower supply the necessary heat to the reboiler of the intermediate-pressure preconcentrator. The overhead vapors of this preconcentrator are, in turn, used to supply the required heat to the reboiler of the lowest-pressure preconcentrator. The bottom product from each preconcentrator is used to preheat the dilute feed. Additional energy savings are accomplished by the appropriate heat exchange between the various feeds, overheads, and bottoms.
机译:用于从发酵或合成原料中回收无水乙醇的热集成萃取蒸馏方法具有四个塔的蒸馏塔。两列是并行运行的预浓缩器。其余的塔是萃取蒸馏脱水塔和夹带剂回收塔。两个预浓缩器和脱水塔在三个相继增加的压力下运行,以使脱水塔的塔顶产物的冷凝蒸气向中压预浓缩器的再沸器提供必要的热量。该预浓缩器的塔顶蒸气又用于向低压预浓缩器的再沸器提供所需的热量。每个预浓缩器的底部产物用于预热稀释的进料。通过在各种进料,塔顶馏出物和塔底物料之间进行适当的热交换,可以进一步节省能源。

著录项

  • 公开/公告号US5035776A

    专利类型

  • 公开/公告日1991-07-30

    原文格式PDF

  • 申请/专利权人 UNIVERSITY OF MASSACHUSETTS;

    申请/专利号US19900502112

  • 发明设计人 JEFFREY P. KNAPP;

    申请日1990-03-29

  • 分类号B01D3/40;

  • 国家 US

  • 入库时间 2022-08-22 05:46:08

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