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TUNGSTEN OXIDE-ANTIMONY PENTOXIDE COMBINED SOL AND PRODUCTION THEREOF
TUNGSTEN OXIDE-ANTIMONY PENTOXIDE COMBINED SOL AND PRODUCTION THEREOF
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机译：氧化钨-锑五氧化二锑复合溶胶及其生产
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摘要
PURPOSE:To improve transparency, refractive index, wear resistance, dyeability and antistatic property by mixing an acidic aq. Sb2O5 sol with a tungstate and adding an amine and carboxylic acid. CONSTITUTION:Potassium antimonate obtd. by allowing Sb2O3 to react with KOH is deionized to obtain an acidic aq. Sb2O5 sol of pH 1-6 having 2-50wt.% concn. of Sb2O5. This sol is mixed with a tungstate such as Na2WO4.2H2O at room temp. to 100 deg.C so that the weight ratio of WO3 to Sb2O5 is regulated to 0.1-1. An amine such as methylamine or the amine and carboxylic acid such as formic acid are added to the mixture by 1-30wt.% of the total amt. of WO3 and Sb2O5 as required. A WO3-Sb2O5 combined sol having 0.1-100 weight ratio of WO3 to Sb2O5 and contg. an alkali metal or ammonium (M) in 0.02-0.7 molar ratio of M2O to WO3+Sb2O5 or further contg. the amine or the amine and carboxylic acid is obtd.
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机译：目的：通过混合酸性水溶液来提高透明度，折射率，耐磨性，可染性和抗静电性能。 Sb2O5溶胶与钨酸盐并加入胺和羧酸。组成：锑酸钾盐。通过使Sb 2 O 3与KOH反应而被去离子以获得酸性水溶液。 pH 1-6的Sb2O5溶胶的浓度为2-50wt。％。的Sb2O5。该溶胶在室温下与钨酸盐如Na2WO4.2H2O混合。到100℃，使得WO 3与Sb 2 O 5的重量比被调节为0.1-1。将胺（例如甲胺）或胺和羧酸（例如甲酸）以混合物总量的1-30wt。％加入混合物中。根据需要制备WO3和Sb2O5。 WO3与Sb2O5的重量比为0.1-100且续的WO3-Sb2O5混合溶胶。 M2O与WO3 + Sb2O5的摩尔比为0.02-0.7的碱金属或铵（M），或进一步续续。禁止使用胺或胺和羧酸。
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