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seen for the purification of ettiksyrahaltig sulphuric acid
seen for the purification of ettiksyrahaltig sulphuric acid
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机译：见于提克西拉哈提格硫酸的提纯
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摘要
Dilute sulfuric acid contaminated with acetic acid and hydrogen chloride is purified with the resultant formation of concentrated sulfuric acid and acetic acid. To this end, the contaminated sulfuric acid is heated in a first step to at most 60 DEG C under 25-30 mm Hg so as to expel all of the hydrogen chloride together with minor proportions of acetic acid and water. In a second step, the sulfuric acid is heated to at most 165 DEG C under 20-25 mm Hg so as to distil off the bulk of acetic acid together with water. In a third step, the sulfuric acid is cooled down to 60 DEG -90 DEG C, diluted with 10-30 wieght % of water with agitation and while cooling is continued. Following this, the sulfuric acid is heated to 160 DEG -165 DEG C under 20-25 mm Hg and thereby freed from the water and residual acetic acid.
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