首页> 外国专利> Device for producing voltage-impulses of short-duration, wherein a discharge-path, which is conductive in a negative direction with respect to the pulses, is connected in parallel with the load

Device for producing voltage-impulses of short-duration, wherein a discharge-path, which is conductive in a negative direction with respect to the pulses, is connected in parallel with the load

机译:用于产生短时电压脉冲的装置,其中,相对于脉冲在负方向上导电的放电路径与负载并联连接

摘要

In the manufacture of regenerated cellulose threads, films and like products from viscose, the cellulose xanthogenate still present in the products after they leave the spinning bath is decomposed by first treating the products with an aqueous solution containing an inorganic acid and at least one inorganic salt, in which the molar ratio of acid to neutral salt is below 1, and thereupon, after freeing the products from the bath liquid, e.g. by washing with water, treating the products with an acid aqueous solution containing no or very little salt. The process is characterized by the first treatment reducing the xanthogenate ratio of the products to about 0.10, by the second treatment taking place at not over 60 DEG C., preferably at room temperature, and by the second treatment being followed by a treatment with steam until the xanthogenate ratio of the products has decreased to 0.003 or less. Finally the products are desulphurized, e.g. by washing with water. The xanthogenate ratio is defined as the ratio of the total number of xanthogenate groups still present in the products to the total number of anhydro-glucose units therein. In the example threads from a spinning bath containing 8 per cent. of sulphuric acid and 14 per cent. of sodium sulphate are passed through a decomposition bath at 80 DEG C. containing 4 per cent. of sulphuric acid and 7 per cent. of sodium sulphate. The threads are stretched about 50 per cent. in this bath, then passed through a water bath at 20 DEG C. and thereafter through a 1 per cent. aqueous sulphuric acid solution at 25 DEG C. The threads are then passed through a long chamber supplied with saturated steam and finally washed with water at 50 DEG C. The low xanthogenate ratio of the thread substance after the treatment with steam enables a more rapid and complete desulphurizing and bleaching of the threads to be accomplished than in prior art processes, and the total steam consumption is reduced. Specification 692,023 is referred to.
机译:在由粘胶纤维制造再生的纤维素线,薄膜等产品时,通过先用含有无机酸和至少一种无机盐的水溶液处理产品,将产品分解后仍存在于产品中的纤维素黄原酸酯分解。 ,其中酸与中性盐的摩尔比小于1,因此,从浴液中释放出产物后,例如通过用水洗涤,用不含或很少盐的酸性水溶液处理产物。该方法的特征在于,第一处理将产物的黄原酸酯比例降低至约0.10,第二处理在不超过60℃,优选在室温下进行,第二处理之后是蒸汽处理。直到产品的黄原酸酯比率降低到0.003或更小。最后将产品脱硫,例如用水冲洗。黄原酸酯比率定义为仍存在于产物中的黄原酸酯基团总数与其中的脱水葡萄糖单元总数的比率。在示例中,纺丝浴中的纱线含量为8%。硫酸和14%。使硫酸钠通过80℃的含有4%的分解浴。硫酸和7%。硫酸钠。线被拉伸约50%。在该浴中,然后通过20℃的水浴,然后再通过1%。在25℃的硫酸水溶液中。然后使线穿过供有饱和蒸汽的长腔室,最后在50℃用水洗涤。在用蒸汽处理后,线状物质的低黄原酸酯比率使得更快和更快速。与现有技术的方法相比,可以完成线的完全脱硫和漂白,并且减少了总蒸汽消耗。参考规范692,023。

著录项

  • 公开/公告号US2736800A

    专利类型

  • 公开/公告日1956-02-28

    原文格式PDF

  • 申请/专利权人 HARTFORD NATIONAL BANK AND TRUST COMPANY;

    申请/专利号US19510204798

  • 发明设计人 BRUIJNING HUGO GEORG;

    申请日1951-01-06

  • 分类号H03K3/55;

  • 国家 US

  • 入库时间 2022-08-23 22:45:05

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