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Preparation method and application of tetragonal NaV2O5⋅H2O nanosheet-like powder

机译:四字环Nav 2 O 5 ⋅H 2 o纳米片状粉末的制备方法和应用

摘要

A preparation method of a tetragonal NaV2O5.H2O nanosheet-like powder includes steps of: (S1) simultaneously adding NaVO3 and Na2S.9H2O into deionized water, and then magnetically stirring, and obtaining a black turbid solution; (S2) sealing after putting the black turbid solution into an inner lining of a reaction kettle, fixing the sealed inner lining in an outer lining of the reaction kettle, placing the reaction kettle into a homogeneous reactor, and then performing a hydrothermal reaction; and (S3) after completing the hydrothermal reaction, naturally cooling the reaction kettle to the room temperature, and then alternately cleaning through water and alcohol, and then collecting a product, drying the product, and finally obtaining the tetragonal NaV2O5.H2O nanosheet-like powder with a thickness in a range of 30-60 nm and a single crystal structure grown along a (002) crystal orientation.
机译:一种制备四边形Nav 2 O 5 .h 2 o纳米片状粉末的方法包括以下步骤:(s1)同时添加navo <将亚> 3 和Na 2 s.9h 2 O进入去离子水,然后磁力搅拌,获得黑色浑浊溶液; (S2)密封在将黑色混浊溶液放入反应水壶的内衬后,将密封内衬在反应釜的外衬里固定,将反应釜置于均相反应器中,然后进行水热反应; (S3)完成水热反应后,自然将反应釜冷却到室温,然后通过水和醇交替清洗,然后收集产品,干燥产品,最后获得四方NAV 2 < /subelyo< sub -5,7/sub`.h] 0-22/sub - 样粉状粉末,厚度在30-60nm的范围内,沿(002)晶体生长的单晶结构方向。

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