首页> 外国专利> METHOD FOR PREPARING ZINC OXIDE QUANTUM DOTS BY ULTRASONIC WAVE ASSISTANCE IN SOLUTE INCOMPLETE DISSOLUTION MODE

METHOD FOR PREPARING ZINC OXIDE QUANTUM DOTS BY ULTRASONIC WAVE ASSISTANCE IN SOLUTE INCOMPLETE DISSOLUTION MODE

机译：通过超声波辅助在溶质不完全溶出模式中用超声波辅助制备氧化锌量子点的方法

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摘要

Provided is a method for preparing zinc oxide quantum dots by ultrasonic wave assistance in solute incomplete dissolution mode, comprising the following steps: step 1: placing zinc-containing inorganic salt in an alcohol organic solvent in an ultrasonic wave environment to form a ZnO precursor suspension A; step 2: fully dissolving strong alkali in the alcohol organic solvent in a stirring environment to obtain a clear solution B; step 3: in the ultrasonic wave environment, adding the clear solution B obtained in step 2 dropwise to the suspension A obtained in step 1, and a full reaction is achieved in the ultrasonic wave environment, the reaction time is 10-40 min to obtain a solution C; step 4: adding the solution C after reaction in step 3 to a nonpolar solvent, carrying out static precipitation, after centrifugation at a certain speed, removing the supernatant, to obtain an initial precipitate, then adding the alcohol organic solvent, and dispersing the precipitate in the ultrasonic wave environment; step 5: repeating step 4 for twice or more to obtain a pure ZnO quantum dot precipitate; step 6, placing the ZnO quantum dot precipitate obtained in step 5 in a vacuum dryer for annealing treatment to obtain ZnO powder.

机译：提供一种通过超声波辅助在溶质不完全溶解模式中用超声波辅助制备氧化锌量子点的方法，包括以下步骤：步骤1：将含锌的无机盐放在超声波环境中的醇有机溶剂中以形成ZnO前体悬浮液一种;步骤2：在搅拌环境中完全溶解在醇有机溶剂中的强碱，得到澄清溶液B;步骤3：在超声波环境中，将在步骤2中获得的透明溶液B滴在步骤1中获得的悬浮液A，并且在超声波环境中实现了完全反应，反应时间为10-40分钟以获得解决方案c;步骤4：在步骤3中反应加入溶液C至非极性溶剂，进行静电沉淀，在一定速度离心后，除去上清液，得到初始沉淀，然后加入醇有机溶剂，并分散沉淀物并分散沉淀物在超声波环境中;步骤5：重复步骤4两次以上以获得纯ZnO量子点沉淀物;步骤6，将步骤5中获得的ZnO量子点沉淀物放置在真空干燥器中，用于退火处理以获得ZnO粉末。

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公开/公告号WO2021082960A1

专利类型
公开/公告日2021-05-06

原文格式PDF
申请/专利权人 INSTITUTE OF LASER AND OPTO ELECTRONICS MANUFACTURING WENZHOU UNIVERSITY;WENZHOU UNIVERSITY;
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申请/专利号WO2020CN121785
发明设计人 ZHONG RONG;ZHOU JIANHUA;SUN HAORAN;QIU CHENGGONG;PAN XIAOMING;ZHENG BEIRONG;WANG YANGBO;
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申请日2020-10-19
分类号C09K11/02;C09K11/54;B82Y30;B82Y20;
国家 CN
入库时间 2022-08-24 18:37:11

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