Methods for making carbon-fiber reinforced geopolymer composites are provided. The methods produce metakaolin-based geopolymer composites in which multiwalled carbon nanotubes and/or carbon nanofibers are well dispersed in an metakaolin-based geopolymer matrix. The mixing protocols of the methods used to produce carbon-fiber reinforced geopolymer composites produce composites with reduced porosity, high elastic moduli, high strength, and/or high fracture toughness.
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