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METHOD FOR QUANTIFYING THE PHASE AMOUNTS OF COMPONENTS OF A CARBONATED ROCK

机译:量化碳酸岩联的分量的量量的方法

摘要

The present disclosure relates to a method for quantifying the phase amounts of a carbonated rock sample comprising the steps of: calibrating a differential thermal analysis, DTA, line from a plurality of quartz references in varying amounts of quartz relative to the total reference amount, with the amount of quartz as a function of the area of endothermic peak quartz inversion; obtaining a DTA area of endothermic peak inversion of the quartz in the sample and calculating the amount of quartz present in the sample using the calibrated DTA line; obtaining an X-ray diffraction, XRD, pattern from the sample; using Rietveld Refinement to fit XRD patterns of crystalline carbonated rock components to the obtained sample XRD pattern, provided that the amount of quartz present in the sample is fixed to be the previously calculated amount; calculating the amounts of the crystalline rock components, other than quartz, from the fitted XRD patterns; calculating a total amount of amorphous and minor phases present in the sample by subtracting the sum of the calculated amounts of the crystalline rock components, including quartz, from the total sample amount.
机译:本公开涉及一种用于量化碳酸岩样品的相位量的方法,包括以下步骤:校准差分热分析,DTA,从多个石英的相对于总参考量的不同量的石英,石英的量作为吸热峰值偏移的面积的函数;获得样品中石英的吸热峰值反演的DTA区域,并使用校准的DTA线计算样品中存在的石英的量;获得X射线衍射,XRD,样品的图案;使用RIETVELD改进将结晶碳酸岩体成分的XRD图案适合于所得的样品XRD图案,只要样品中存在的石英量固定为先前计算的量;从装配的XRD图案计算除石英的结晶岩石部件的量;通过从总样品量减去包括石英的计算量的计算量的总和计算样品中存在的无定形和次要相的总量。

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