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DEFECTS IN FINE-GRAINED AND POROUS MATERIALS CHARACTERIZED BY POSITRON ANNIHILATION

机译:正电子NI没表征的细颗粒和多孔材料中的缺陷

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摘要

We investigate the annihilation parameters (lifetimes and intensities) for positrons becoming trapped at grain boundaries and at inner surfaces (pores), examining fine-grained nickel powder compacts (effective powder particle size 1 ― 10 μm with grains in or even below the micron size). Furthermore, we can monitor grain growth and sintering (volume shrinkage) during successive heat treatment of powder compacts. To reach this aim, we correlate the annihilation parameters with results of a Monte-Carlo simulation and analytical solutions of the positron diffusion. We find that it is possible to determine an effective average powder particle size as well as grain sizes by positron lifetime spectroscopy.
机译:我们研究了正电子被困在晶界和内表面(孔)时的the没参数(寿命和强度),检查了细颗粒的镍粉压块(有效粉末粒度为1〜10μm,晶粒为微米甚至小于微米) )。此外,我们可以监测粉末压坯的连续热处理过程中的晶粒长大和烧结(体积收缩)。为了达到这个目的,我们将the没参数与蒙特卡洛模拟的结果和正电子扩散的解析解相关联。我们发现有可能通过正电子寿命光谱法确定有效的平均粉末粒径以及晶粒尺寸。

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