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首页> 外文会议>The American Institute of Chemical Engineers 2002 Spring National Meeting, Mar 10-14, 2002, New Orleans, LA >Use Continuous Lab Scale Unit for Direct Scale-Up of Commercial Polymerization Process
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Use Continuous Lab Scale Unit for Direct Scale-Up of Commercial Polymerization Process

机译：使用连续实验室规模装置直接放大商业聚合工艺

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摘要

An automated lab reactor is utilized as continuous stirred tank reactor to develop and optimize a bench scale polymerization process. Statistical experimental designs are employed to identify the critical variables, and to screen effects and interactions. The acquired operating data are optimized to create the design for a plant polymerization process. Excellent correlation of the bench and plant scale mathematical models demonstrates that no intermediate pilot plant scale-up is necessary. The identity of monomer, catalysts, reagents, solvent and reaction mechanisms are proprietary, and are not disclosed in this presentation. This miniature polymerization pilot plant was presented by the author at the AlChE National Spring Meeting, March 11-14, 2002, in New Orleans, Louisiana.
机译：自动化实验室反应器用作连续搅拌釜反应器，以开发和优化台式规模的聚合工艺。统计实验设计用于识别关键变量，并筛选效果和相互作用。优化所获取的操作数据以创建用于工厂聚合过程的设计。实验台和工厂规模数学模型之间的出色关联表明，无需进行中间试验工厂规模扩大。单体，催化剂，试剂，溶剂和反应机理的身份是专有的，在本演示中未公开。作者在2002年3月11日至14日在路易斯安那州新奥尔良举行的AlChE全国春季会议上介绍了这种微型聚合试验工厂。

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