Synthesis and Characterization of Nanosize Molybdenum Disulfide Particles by Quick Homogeneous Precipitation Method

机译：快速均相沉淀法合成和表征纳米二硫化钼颗粒

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Molybdenum sulfide nanoparticles were prepared via quick homogeneous precipitation method (QHPM) by the reaction between Na_2MoO_4 and CH_3CSNH_2 in the presence of sulfuric acid at 80℃. The as-synthesized molybdenum sulfide particles were studied by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM). The results showed that the as-synthesized molybdenum sulfide was amorphous MoS_3 nanoparticles with an average size of 40 nm. The resultant amorphous MoS_3 nanoparticles were then calcined under hydrogen gas flow at a selected temperature for 50 minutes. The results of XRD, TEM, and HRTEM confirmed that the MoS_2 nanoparticles with about 40 nm were prepared from the amorphous M0S3 nanoparticles at 780 ℃.

机译：Na_2MoO_4与CH_3CSNH_2在80℃的硫酸存在下，通过快速均相沉淀法（QHPM）制备了硫化钼纳米颗粒。通过X射线粉末衍射（XRD），透射电子显微镜（TEM）和高分辨率透射电子显微镜（HRTEM）研究了合成的硫化钼颗粒。结果表明，所合成的硫化钼为非晶态的MoS_3纳米粒子，平均粒径为40 nm。然后将所得的非晶态MoS_3纳米颗粒在氢气流中于选定的温度下煅烧50分钟。 XRD，TEM和HRTEM的结果证实，在780℃下由无定形的MoS3纳米粒子制备了约40nm的MoS_2纳米粒子。

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《Asian Pacific Conference on Fracture and Strength;APCFS; 20061122-25;20061122-25; Sanya(CN);Sanya(CN)》|2006年|P.21072110|共2页
会议地点 Sanya(CN);Sanya(CN)
作者
Kunhong HU; Xianguo HU; Xiaojun SUN; Hefeng JING; Song ZHAN;
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作者单位

School of Mechanical and Automotive Engineering, Hefei University of Technology,Hefei 230009, China;

Department of Chemistry and Materials Engineering, Hefei University, Hefei 230022, China;

State Key Laboratory of Solid Lubrication, Lanzhou Institute of C;

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原文格式 PDF
正文语种 eng
中图分类机械试验法;
关键词
quick homogenous precipitation method; molybdenum disulfide; MoS_2 nanoparticles;

机译：快速均匀沉淀法;二硫化钼; MoS2纳米粒子;

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专利

1. Synthesis and Characterization of Nanosize Molybdenum Disulfide Particles by Quick Homogeneous Precipitation Method [J] . Kunhong HU, Xianguo HU, Xiaojun SUN, Key Engineering Materials . 2007,第Pt3期

机译：快速均相沉淀法合成和表征纳米二硫化钼颗粒
2. Synthesis of Nanosized Tin Oxide (SnO_2) Particles via Homogeneous Precipitation [J] . OE. Acarbas, E. Suvaci, A. Dogan Key Engineering Materials . 2004,第Pt2期

机译：均相沉淀法合成纳米氧化锡（SnO_2）颗粒
3. Synthesis and Characterization of Uniform Zirconia Particles by Homogeneous Precipitation Method [J] . Khalida Akhtar, Ikram Ul Haq, Uzma Hira High temperature materials and processes . 2013,第4期

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4. Synthesis and Characterization of Nanosize Molybdenum Disulfide Particles by Quick Homogeneous Precipitation Method [C] . Kunhong HU, Xianguo HU, Xiaojun SUN, Asian Pacific Conference on Fracture and Strength . 2007

机译：快速均相沉淀法的纳米氧化钼颗粒的合成与表征
5. Synthesis of silver nanoparticles integrated molybdenum disulfide nanoparticles and fundamental understanding the behavior of silver-molybdenum disulfide nanoparticles based hybrid system. [D] . Zhang, Wenyang. 2010

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Synthesis and Characterization of Nanosize Molybdenum Disulfide Particles by Quick Homogeneous Precipitation Method

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