INTERCALATION OF POTASSIUM INTO FULLERITE C_(60): ~(13)C AND ~(39)K NMR DATA

机译：钾到富勒石C_（60）中的嵌入：〜（13）C和〜（39）K NMR数据

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The K - C_(60) system was studied using the NMR method. The phase composition of the sample with the empirical formula K_1C_(60) was determined; K_1C_(60), K_3C_(60), a solid solution of K in fullerite C60, and polymer were detected and their amounts were estimated. The maximal content of polymer was not more than 90%. In samples with different contents of K_3C_(60), solid solution, and polymer, the ratio of occupancies of tetrahedral and octahedral sites with potassium was found to be 2 : 1.

机译：使用NMR方法研究了K-C_（60）系统。确定具有经验公式K_1C_（60）的样品的相组成；检测K_1C_（60），K_3C_（60），K在富勒石C60中的固溶体和聚合物，并估计它们的量。聚合物的最大含量不超过90％。在具有不同K_3C_（60），固溶体和聚合物含量的样品中，发现四面体和八面体位点与钾的比率为2：1。

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来源
《Fullerenes and Nanotubes: The Building Blocks of Next Generation Nanodevices: Fullorenes》|2003年|P.509-517|共9页
会议地点 Paris(FR);Paris(FR);Paris(FR)
作者
E.V. Skokan; V.P. Tarasov; V.I. Privalov; V.E. Aleshina; Yu.B. Muravlev; I.V. Arkhangelskii;
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Department of Chemistry, Moscow State University, Moscow, 119899, Russia;

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原文格式 PDF
正文语种 eng
中图分类无机高分子化合物（高聚物）;
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1. Hartree-Fock crystal orbital calculation on sodium-intercalated fullerites C_(60)Na_(10) and C_(60)Na_(11) [J] . E. B. Starikov Chemical Physics: A Journal Devoted to Experimental and Theoretical Research Involving Problems of Both a Chemical and Physical Nature . 2000,第2期

机译：钠插层富铝C_（60）Na_（10）和C_（60）Na_（11）的Hartree-Fock晶体轨道计算
2. Spin-Lattice Relaxation and ~(13)C NMR Line Shape at Multiaxial Reorientation of Molecules in Fullerite C_(60) [J] . Dmitry E. Izotov, Valerii P. Tarasov The journal of physical chemistry, B. Condensed matter, materials, surfaces, interfaces & biophysical . 2002,第21期

机译：富勒石C_（60）中分子多轴重取向时的自旋晶格弛豫和〜（13）C NMR线形
3. Orientational phase transition in methane-intercalated fullerite C_(60) [J] . Skokan E. V, Shulga Yu M., Troyanov S. I Physical review. B, Condensed Matter And Materals Physics . 2018,第21期

机译：甲烷插层富勒石C_（60）的取向相变
4. Intercalation of fullerite C_(60) with Potassium:~(13)C and ~(39)K NMR data [C] . E.V.Skokan, V.P.Tarasov, V.I.Privalov, The Meeting of the Electrochemical Society . 2003

机译：与钾的静态C_（60）嵌入：〜（13）C和〜（39）K NMR数据
5. Practicum Three, August 2000. Novel applications of carbon-13 indirect detection NMR to metabolic tracer studies in small tissue samples. Practicum Two, December 1998. Proton and platinum-195 NMR spectroscopic characterization of the products formed in reactions of N-isobutyramide-Gly-Phe-Leu-Gly-ethylenediamine and similar model ligands with potassium tetrachloroplatinate (II). Practicum One, August 1997. Synthesis of a polyamide containing repeating macrocyclic chelate units: Evaluation of its gadolinium(3+) complex as a MRI contrast agent. [D] . Burgess, Shawn C. 2000

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7. ~(13)C NMR谱和一些C_(60)衍生物结构探讨 [O] . 乃兴王 1995

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8. Potent Solvents for C60 and their Utility for the Rapid Acquisition of 13CNMRData for Fullerenes [R] . Scrivens, W. A., Tour, J. M. 1993

机译：用于C60的强效溶剂及其用于快速获取富勒烯的13CNmR数据的实用程序

INTERCALATION OF POTASSIUM INTO FULLERITE C_(60): ~(13)C AND ~(39)K NMR DATA

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