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Effect of Preparation Conditions of Activated Carbon from Corn Cob by Chemical Activation with Microwave Energy

机译:微波化学活化玉米芯制备活性炭条件的影响

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The conditions for the preparation of activated carbon(AC) from corn cob(CC) treated with NaHCO3 using microwave radiation were optimized through response surface methodology (RSM) and central composite design (CCD). The effects of the radiation power, radiation time, and impregnation ratio were studied from the adsorption capacity on methylene blue dye(MB), and yield results. From the analysis of variance (ANOVA), the most influential factor on each experimental design response was identified. The predicted MB adsorption capacity and yield after process optimization was found to agree satisfactory with the experimental values. The optimum conditions for preparing AC from CC were found as follows: radiation power of 572W, radiation time of 5 min and impregnation ratio of 3.18. The predicted and experimental results for the adsorption capacity on MB and yield of AC were 263mg/g ¡¢24.9% and 251mg/g¡¢26.2%, respectively.
机译:通过响应面法(RSM)和中心复合设计(CCD)优化了用NaHCO3处理的玉米芯(CC)微波辐射制备活性炭(AC)的条件。从对亚甲基蓝染料(MB)的吸附容量研究了辐射功率,辐射时间和浸渍率的影响,并得出了收率。通过方差分析(ANOVA),确定了每个实验设计响应中最有影响力的因素。发现工艺优化后预测的MB吸附容量和产率与实验值相符。发现由CC制备AC的最佳条件如下:辐射功率为572W,辐射时间为5分钟,浸渍比为3.18。对MB的吸附量和AC收率的预测和实验结果分别为263mg / g±24.9%和251mg / g±26.2%。

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