首页> 外文会议>ICT International Annual Conference >Preparation and Solid State ~(13)C-NMR of the Four Stable Phases of 2,4,6,8,10,12-Hexanitro-2,4,6,8,10,12-hexaazatetracyclo5.5.0.0~(5.9).0~(3,11)dodecane (HNIW, CL 20)

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Preparation and Solid State ~(13)C-NMR of the Four Stable Phases of 2,4,6,8,10,12-Hexanitro-2,4,6,8,10,12-hexaazatetracyclo5.5.0.0~(5.9).0~(3,11)dodecane (HNIW, CL 20)

机译：制备和固态〜（13）C-NMR的四个稳定相2,4,6,8,12-12-己酸-2,4,6,8,10,12-六己酰谱5.5.0.0〜（ 5.9）.0〜（3,11）十二烷（HNIW，CL 20）

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CL 20 was prepared in a four step synthesis by a variation of Nielsen's classical method. This produced the alpha hydrated phase of CL 20. The other polymorphs were prepared by solution/precipitation in selected solvent/non-solvent pairs. The phase transitions obtained were alpha to beta, beta to gamma and beta to epsilon. FT-IR spectra of some polymorphs were recorded. Solid state ~(13)C NMR was done under cross polarisation conditions with magic angle spinning and a tentative assignment of the signals was attempted.

机译：通过尼尔森的经典方法的变化，在四步合成中制备了Cl 20。这产生了Cl 20的α水合相。通过选定的溶剂/非溶剂对中的溶液/沉淀制备其它多晶型物。获得的相转变是α至β，β至γ和β至ePsilon。记录了一些多晶型物的FT-IR光谱。固态〜（13）C NMR在具有魔法角旋转的交叉偏振条件下进行，并尝试暂定分配信号。

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《ICT International Annual Conference》|2006年||共10页
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Manfred Kaiser; Lee Yiew Wang; Patrick Goede; Fraunhofer-Institut fur Chemische Technologie(ICT);
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中图分类爆炸物工业、火柴工业;
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1. Fourier Transform Raman Spectroscopy of the Four Crystallographic Phases of alpha,beta,gamma and epsilon 2,4,6,8,10,12-Hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0~(5,9),0~(3,11)]dodecane (HNIW,CL-20) [J] . Patrick Goede, Nikolaj V.Latypov, Henric Ostmark Propellants, Explosives, Pyrotechnics . 2004,第4期

机译：α，β，γ和ε四个晶体相2,4,6,8,10,12-六硝基-2,4,6,8,10,12-六氮杂四环的傅立叶变换拉曼光谱[5.5.0.0〜（ 5,9），0〜（3,11）]十二烷（HNIW，CL-20）
2. Crystal structure of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0(5.9).0(3.11)] dodecane 1/3 hydrate, C6H8N12O13 [J] . Yu Yuehai, Jin Shaohua, Zhu Jiaping, Zeitschrift fur Kristallographie. New crystal structures . 2016,第2期

机译：2,4,6,8,10,12-六硝基-2,4,6,8,10,12-六氮杂四环[5.5.0.0（5.9）.0（3.11）]十二烷1/3水合物的晶体结构，C6H8N12O13
3. CRYSTAL STRUCTURE OF COCRYSTALS 2,4,6,8,10,12-HEXANITRO-2,4,6,8,10,12-HEXAAZATETRACYCLO [5.5.0.0~(5.9).0~(3.11)]DODECANE WITH 7Н-TRIS-1,2,5-OXADIAZOLO (3,4-b:3′,4′-d:3″,4″-f) AZEPINE [J] . S. M. Aldoshin, Z. G. Aliev, T. K. Goncharov, Journal of structural chemistry . 2014,第2期

机译：晶体2,4,6,8,10,12-己二酸-2,4,6,8,10,12-己二酸TRACYCLO的晶体结构[5.5.0.0〜（5.9）.0〜（3.11）]具有7Н-的十二烷TRIS-1,2,5-OXADIAZOLO（3,4-b：3'，4'-d：3″，4″ -f）氮丙啶
4. Preparation and Solid State ~(13)C-NMR of the Four Stable Phases of 2,4,6,8,10,12-Hexanitro-2,4,6,8,10,12-hexaazatetracyclo5.5.0.0~(5.9).0~(3,11)dodecane (HNIW, CL 20) [C] . Manfred Kaiser, Lee Yiew Wang, Patrick Goede, ICT International Annual Conference . 2006

机译：制备和固态〜（13）C-NMR的四个稳定相2,4,6,8,12-12-己酸-2,4,6,8,10,12-六己酰谱5.5.0.0〜（ 5.9）.0〜（3,11）十二烷（HNIW，CL 20）
5. The Crystal Structure and Morphology of 2,4,6,8,10,12-Hexanitro-2,4,6,8,10,12-hexaazaisowurtzitane (CL-20) p-Xylene Solvate: A Joint Experimental and Simulation Study [O] . Fanfan Shen, Penghao Lv, Chenghui Sun, 2014

机译：2,4,6,8,10,12-六硝基-2,4,6,8,10,12-六氮杂异纤锌矿型结构烷烃（CL-20）对二甲苯溶剂化物的晶体结构和形态：联合实验和模拟研究

Preparation and Solid State ~(13)C-NMR of the Four Stable Phases of 2,4,6,8,10,12-Hexanitro-2,4,6,8,10,12-hexaazatetracyclo5.5.0.0~(5.9).0~(3,11)dodecane (HNIW, CL 20)

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