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The Effect of Alkalization Treatment on Fiber-Matrix Compatibility in Natural Fiber Reinforced Composite

机译:碱化处理对天然纤维增强复合材料纤维 - 基质相容性的影响

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This work was aimed to investigate the effect of alkalization treatment on the fiber-matrix interfacial interaction and hence their compatibility. Kenaf fiber was treated using a 6% NaOH solution for 8 hours. The composites were produced by mixing the treated fiber with PP at various temperatures, duration, and fiber composition. Alteration on the surface chemistry of the fiber was identified by performing FTIR analysis. The surface energy of the treated fiber was mathematically derived from the contact angle measurement results. The compatibility level between treated fiber and PP matrix was visualized through FESEM analysis. Tensile strength tests were also conducted to obtain data necessary for exploring the relationship between the thermodynamic aspects of the fiber-matrix interfacial interaction and the mechanical properties of the composites. The FTIR spectra show that there was significant increase in the %transmittance at wavelength range of 3100-3600 cm-1 indicating that O-H groups were degraded during treatment. However, the polar component of the surface energy for treated fiber was instead higher compared to the untreated one. The SEM images show that there are no noticeable reduction in the size of the treated fibers as expected. On the other hand, the tensile strength of the PP-treated fibers composites reached its highest value when the matrix were loaded with fibers at the lowest percentage i.e. 5%.
机译:这项工作旨在探讨碱化处理对纤维基质界面相互作用,因此其相容性的作用。洋麻纤维使用6%的NaOH溶液处理8小时。该复合材料是通过在不同温度下,持续时间,和纤维组分与PP的处理过的纤维混合而产生。在纤维的表面化学性质改变的鉴定通过进行FTIR分析。处理过的纤维的表面能量从数学上的接触角测量结果的。处理过的纤维和PP基体之间的相容性水平通过FESEM分析显现。还进行了拉伸强度测试,以获得必要探索纤维 - 基体界面相互作用的热力学方面和复合材料的机械性能之间的关系的数据。 FTIR谱表明,在波长范围内的3100-3600厘米-1表示-O-H基团治疗期间被降解的%透光率显著增加。然而,用于处理的纤维的表面能的极性分量代替较高比未经处理的一个。该SEM图像表明,在处理过的纤维的尺寸没有明显的减小预期。在另一方面,当基体在最低百分比即5%装载有纤维PP处理纤维复合材料的拉伸强度达到其最高值。

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