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Nanofiber Formation in Spider Dragline-Silk as Probed by Atomic Force Microscopy and Molecular Pulling

机译：蜘蛛爪线 - 丝绸中的纳米纤维形成如原子力显微镜探测和分子拉动

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Despite the extensive interest in its remarkable materials properties,the structure of spider dragline silk is not yet known.Indirect structural information is thus of particular interest.New data are presented here from two probe microscopy techniques-atomic force microscopy (AFM) and single-molecule force spectroscopy,or 'molecular pulling.'Using a soluble synthetic protein from dragline silk,segmented silk nanofibers have been observed by AFM.Molecular pulling (Force Spectroscopy) has revealed sawtooth-like rupture peaks,indicative of the sacrifical bonds and hidden lengths seen in molecules of other self-healing biometerials.A model is presented for the folding of single dragline-silk molecules and the arangement of these molecules into nanofibers.The relationship is discussed between these molecular/nanoscale results and the materials properties of natural and artificial dragline silks.

机译：尽管对其显着材料的性质进行了广泛的兴趣，但尚未知道蜘蛛龙丝的结构。因此，载体结构信息是特别的兴趣。这里从两种探针显微镜技术 - 原子力显微镜（AFM）和单一 - 分子力谱或“分子拉伸。通过AFM观察到来自拖拉丝的可溶性合成蛋白，通过AFM .MOM分子拉动（力光谱）透露了锯齿状的破裂峰，表示牺牲粘接和隐藏长度在其他自我愈合的学生分子中看到的。提出了一种模型，用于折叠单次鳞片丝分子，并将这些分子的折叠成纳米纤维。这些分子/纳米级结果与自然和人工的材料性质之间讨论了关系拖拉丝网。

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《Materials Research Society Symposium》|2003年||共7页
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Emin Oroudjev; Cheryl Y.Hayashi; Jason Soares; Steven Arcidiiacono; Stephen A.Fossey; Helen G.Hansma;
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中图分类工程材料学;
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专利

1. Contact mechanics modeling of pull-off measurements: Effect of solvent, probe radius, and chemical binding probability on the detection of single-bond rupture forces by atomic force microscopy [J] . Skulason H., Frisbie CD. Analytical chemistry . 2002,第13期

机译：剥离测量的接触力学模型：溶剂，探针半径和化学键合概率对原子力显微镜检测单键断裂力的影响
2. An Atomic Force Microscopy Study on Self-assembled Monolayers of Fluorinated Thiols and Disulfides on Polycrystalline Gold: Implications of the Mechanical Stability, Molecular Order, Pull-off Forces and Frictional Properties for Application in Chemic [J] . H. Schonhorr, G. J. Vancso Polymer Preprints . 1996,第2期

机译：多晶金上氟化硫醇和二硫化物自组装单分子层的原子力显微镜研究：机械稳定性，分子序，拉脱力和摩擦学性质在化学中的应用意义
3. Label-free DNA detection platform based on atomic force microscopy visualisation: characterising the molecular-recognition-triggered conformational changes of an immobilised receptor oligonucleotide probe [J] . Koji Nakano, Hirokazu Yamanouehi, Hisao Yoshinaga, Chemical Communications . 2010,第31期

机译：基于原子力显微镜可视化的无标记DNA检测平台：表征固定的受体寡核苷酸探针的分子识别触发的构象变化
4. Nanofiber Formation in Spider Dragline-Silk as Probed by Atomic Force Microscopy and Molecular Pulling [C] . Emin Oroudjev, Cheryl Y.Hayashi, Jason Soares, Materials Research Society Symposium . 2003

机译：蜘蛛爪线 - 丝绸中的纳米纤维形成如原子力显微镜探测和分子拉动
5. Exploring Atomic Force Microscopy To Probe Charge Transport Through Molecular Films And For The Development Of Combinatorial Force Microscopy. [D] . Chisholm, Roderick A. 2011

机译：探索原子力显微镜以探测通过分子膜的电荷传输并开发组合力显微镜。
6. Colloquium Paper: Segmented nanofibers of spider dragline silk: Atomic force microscopy and single-molecule force spectroscopy [O] . E. Oroudjev, J. Soares, S. Arcidiacono, 2002

机译：讨论会论文：蜘蛛式拉铲丝的分段纳米纤维：原子力显微镜和单分子力谱
7. Segmented nanofibers of spider dragline silk: Atomic force microscopy and single-molecule force spectroscopy [O] . Oroudjev, E., Soares, J., Arcidiacono, S., 2002

机译：蜘蛛拉延丝的分段纳米纤维：原子力显微镜和单分子力谱
8. Probing Redox-Induced Molecular Transformations by Atomic-Resolution ScanningTunneling Microscopy: Iodide Adsorption and Electrooxidation on Au(111) in Aqueous Solution [R] . Gao, X., Weaver, M. J. 1992

机译：原子分辨率扫描隧道显微镜检测氧化还原诱导的分子转化：水溶液中au（111）上碘的吸附和电氧化

Nanofiber Formation in Spider Dragline-Silk as Probed by Atomic Force Microscopy and Molecular Pulling

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