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Fabrication and Characterization of Poly(vinyl alcohol)/ Functionalized Graphene Oxide Nanofibers Produced by Electrospinning Method

机译:通过电刺绣方法制备聚(乙烯醇)/官能化石墨烯氧化物纳米纤维的制备和表征

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A series of poly (vinyl alcohol) (PVA)/functionalized graphene oxide (FGO) nanofibers with low feeding ratios of FGO to PVA were fabricated by electrospinning method. In this study, the prepared PVA/FGO nanocomposites were dispersed in water phase followed by electrospinning treatment under different operational parameters (i.e., applied voltage, feeding rate and FGO contents) to give nanofibers of various diameters and morphologies. The morphology, diameter and structure of electrospun nanofibers and FGO were investigated by Fourier transform infrared (FT-IR) spectroscopy, X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), (TGA) and differential scanning calorimetry (DSC). SEM images showed that the morphologies of the nanofibers were improved by the incorporation of FGO at a low loading content (e.g., 0.1-0.5 wt %) as compared to pure electrospun PVA. The crystallinity and thermal stability of PVA/FGO nanofibers were also studied.
机译:通过静电纺丝法制造了一系列具有低进料比FGO对PVA的乙烯醇/官能化的石墨烯氧化物(FGO)纳米纤维。在该研究中,将制备的PVA / FPO纳米复合材料分散在水相中,然后在不同的操作参数(即,施加的电压,喂料速率和FPO含量)下进行静电处理,得到各种直径和形态的纳米纤维。通过傅里叶变换红外(FT-IR)光谱,X射线光电子体光谱(XPS),扫描电子显微镜(SEM),透射电子显微镜(TEM),X射线,X射线,研究了Electrom Orthop纳米纤维和FGO的形态,直径和结构。衍射(XRD),(TGA)和差示扫描量热法(DSC)。 SEM图像显示,与纯Electrom OperPVA相比,通过在低负载率(例如,0.1-0.5wt%)中,通过掺入FGO来改善纳米纤维的形态。研究了PVA / FPO纳米纤维的结晶度和热稳定性。

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