Application of a mixture of Oxidized Multi-walled Carbon Nanotubes and D-(-)-tartaric Acid-impregnated Silica Gel as Stationary Phases for Thin-layer Chromatographic Enantioseparation

机译：将氧化多壁碳纳米管和D - （ - ） - 酒酸浸渍硅胶混合物的施用在薄层色谱肾上腺素映射分析中的固定相

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The oxidized multi-walled carbon nanotubes were prepared by a nitric acid treatment procedure, which were then used as additive in thin-layer chromatography stationary phases for resolution of ofloxacin, mandelic acid and 2-chloro-mandelic acid enantiomers. In a sharp contrast with pristine multi-walled carbon nanotubes/D-(-)-tartaric acid impregnated thin-layer chromatography plates, oxidized multi-walled carbon nanotubes/D-(-)-tartaric acid impregnated plates presented better enantioseparation effects for ofloxacin enantiomers.

机译：通过硝酸处理程序制备氧化的多壁碳纳米管，然后用作薄层色谱法的添加剂，用于分离氧氟沙星，扁桃酸和2-氯仙甲酸对映体。与原始多壁碳纳米管/ D - （ - ） - 酒石酸浸渍的薄层色谱板鲜明对比，氧化多壁碳纳米管/ D - （ - ） - 酒石酸浸渍板对氧氟沙星的更好的映对映对映对作用对映体。

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来源
《International Conference on Materials and Products Manufacturing Technology》|2013年||共3页
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作者
Zhi Guang Peng; Dong Hong Yin; Jian Fu Liu; Jin Gang Yu; Xiao Na Yang; Dong Ming Zeng;
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原文格式 PDF
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中图分类 TB3-532;
关键词
Oxidized Multi-walled Carbon Nanotubes; Enantioseparation; Ofloxacin; Thin-layer Chromatography;

机译：氧化多壁碳纳米管;映上分离;氧氟沙星;薄层色谱;

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1. High-performance liquid chromatographic enantioseparation of (R,S)-fluoxetine using Marfey's reagent and (S)-N-(4-nitrophenoxycarbonyl) phenylalanine methoxyethyl ester as chiral derivatizing reagents along with direct thin-layer chromatographic resolution and isolation of enantiomers using L-tartaric acid as mobile phase additive. [J] . Bhushan R, Agarwal C Biomedical Chromatography: An International Journal Devoted to Research in Chromatographic Methodologies and Their Applications in the Biosciences . 2010,第11期

机译：使用Marfey's试剂和（S）-N-（4-硝基苯氧基羰基）苯丙氨酸甲氧基乙基酯作为手性衍生试剂，对（R，S）-氟西汀进行高效液相色谱对映分离，并使用L对映体进行直接薄层色谱分离和分离-酒石酸作为流动相添加剂。
2. Multi-Walled Carbon Nanotubes Mediated Thin-Layer Chromatographic Enantioseparation of Ofloxacin [J] . Dushu Huang, Jingang Yu, Wei Liu, Current Nanoscience . 2013,第1期

机译：多壁碳纳米管介导氧氟沙星的薄层色谱对映体分离
3. In situ synthesis of monolithic molecularly imprinted stationary phases for liquid chromatographic enantioseparation of dibenzoyl tartaric acid enantiomers [J] . Xiaoqing Chen, Weijie Yang, Yangmeihui Zhou, Journal of porous materials . 2012,第5期

机译：原位合成单分子印迹固定相，用于二苯甲酰基酒石酸对映体的液相色谱对映分离
4. Application of a mixture of Oxidized Multi-walled Carbon Nanotubes and D-(-)-tartaric Acid-impregnated Silica Gel as Stationary Phases for Thin-layer Chromatographic Enantioseparation [C] . Zhi Guang Peng, Dong Hong Yin, Jian Fu Liu, International Conference on Materials and Products Manufacturing Technology . 2013

机译：将氧化多壁碳纳米管和D - （ - ） - 酒酸浸渍硅胶混合物的施用在薄层色谱肾上腺素映射分析中的固定相
5. Development of a sol-gel-based thin-layer chromatography stationary phase for in-situ infrared analysis [D] . Jones, Linda Kay 2008

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6. Immobilization of Chondroitin Sulfate A onto Monolithic Epoxy Silica Column as a New Chiral Stationary Phase for High-Performance Liquid Chromatographic Enantioseparation [O] . Ratih Ratih, Hermann Wätzig, Azminah Azminah, 2021

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机译：化学键合到硅胶上的核黄素衍生物的对映体分离，作为HPLC的手性固定相

Application of a mixture of Oxidized Multi-walled Carbon Nanotubes and D-(-)-tartaric Acid-impregnated Silica Gel as Stationary Phases for Thin-layer Chromatographic Enantioseparation

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