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Multiwall Carbon Nanotubes-modified Glassy Carbon Electrode for Square-wave Stripping Voltammetric Determination of Aqueous Antimony (III) ion

机译:用于方波剥离伏安法测定水性锑(III)离子的多壁碳纳米管改性玻碳电极

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A glassy carbon electrode (GCE) modified with multiwall carbon nanotubes (MWCNTs) for electrochemical square-wave stripping voltammetric (SWV) determination of antimony (III) was introduced. Various experimental parameters, such as the amounts of carbon nanotubes, the deposition potential and time, the electrolyte solution, etc, were thoroughly optimized and discussed. Under the optimum experimental conditions, the MWCNTs-modified GCE exhibited well linear behaviour in the antimony(III) concentration range from 0.04 to 0.26 mg/L (R=0.9983) with a detection limit of 3.20×10~(-4) mg/L (S/N=3) under a 360 s accumulation. The proposed electrode also exhibited encouraging properties for measurements of simulated water samples.
机译:用多壁碳纳米管(MWCNT)改性用于电化学方波剥离伏安(SWV)的玻璃碳电极(GCE),介绍了锑(III)的锑(III)的测定。各种实验参数,例如碳纳米管的量,沉积电位和时间,电解质溶液等被彻底优化和讨论。在最佳实验条件下,MWCNTS改性的GCE在锑(III)浓度范围内显示出良好的线性行为范围为0.04至0.26mg / L(r = 0.9983),检测限为3.20×10〜(-4)mg / L(s / n = 3)在360秒的累积下。所提出的电极还表现出令人促进模拟水样的测量的性质。

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