Experimental Studies of Catalytic Hydrogenation of Isophthalonitrile for Meta-Xylenediamine Preparation

机译：荟萃二甲二胺制剂中邻苯二甲腈催化氢化的实验研究

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With Raney nickel catalyst, the process of catalytic hydrogenation of isophthalonitrile for meta-xylenediamine preparation using aniline as the solvent is studied in this paper. The effect of the amount of catalyst, the reaction pressure and temperature is discussed. The results show that: on the conditions of the initial raw materials concentration for 2.0mol/L, the ratio of the catalyst quality and the IPN quality for 1/10, the reaction temperature for 100°C, the reaction pressure for 35bar, the reaction inhibitor NaOH for 0.6g and some additives, the reaction is conducted for 80min and the quality yield of meta-xylenediamine is up to 98.58%.

机译：用阮内镍催化剂，本文研究了使用苯胺作为苯胺进行苯胺 - 二甲双二胺制备的邻苯二甲腈的催化氢化方法。讨论了催化剂量，反应压力和温度的影响。结果表明：在初始原料浓度的条件下为2.0mol / L，催化剂质量的比例和1/10的IPN质量，反应温度100°C，反应压力为35bar，反应抑制剂NaOH 0.6g和一些添加剂，对反应进行80分钟，元 - 二甲二胺的质量收率高达98.58％。

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《International Conference on Materials Science and Engineering Technology》|2014年||共5页
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作者
Yugang Li;
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中图分类 TB3-53;
关键词
Meta-xylenediamine (MXDA）; Isophthalonitrile (IPN）; Hydrogenation; Catalyze;

机译：Meta-X二甲二胺（MXDA）;邻苯二甲腈（IPN）;氢化;催化;

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专利

1. Catalytic hydrogenation of isophthalonitrile (IPN) over supported monometallic and bimetallic catalysts [J] . Liu Chang, Li Xiaodan, Wang Tiefeng RSC Advances . 2015,第71期

机译：负载型单金属和双金属催化剂上的间苯二甲腈（IPN）催化加氢
2. EFFECT OF REACTION SOLVENT ON THE HYDROGENATION OF ISOPHTHALONITRILE FOR META-XYLYLENDIAMINE PREPARATION [J] . Sung Wook Row, Tae Young Chae, Kye Sang Yoo The Canadian Journal of Chemical Engineering . 2007,第6期

机译：反应溶剂对异戊二腈加氢制备间二甲苯二胺的影响
3. Study on the Preparation of Biohydrocarbon Fuel by Catalytic Hydrogenation of Swida wilsoniana Pyrolysis Products [J] . Aihua Zhang, Juan Tang, Jilie Lie, Advances in materials science and engineering . 2020,第9期

机译：Swida Wilsoniana热解产物催化氢化制备生物氢碳燃料的研究
4. Experimental Studies of Catalytic Hydrogenation of Isophthalonitrile for Meta-Xylenediamine Preparation [C] . Yugang Li International Conference on Materials Science and Engineering Technology . 2014

机译：荟萃二甲二胺制剂中邻苯二甲腈催化氢化的实验研究
5. Preparation of palladium containing cubic mesoporous materials and their application towards catalytic hydrogenation reactions. [D] . Balasanthiran, Vagulejan. 2010

机译：含钯的立方介孔材料的制备及其在催化加氢反应中的应用。
6. Characterization of the hydrolytic activity of a polyclonal catalytic antibody preparation by pH-dependence and chemical modification studies: evidence for the involvement of Tyr and Arg side chains as hydrogen-bond donors. [O] . M Resmini, R Vigna, C Simms, 1997

机译：通过pH依赖性和化学修饰研究表征多克隆催化抗体制剂的水解活性：Tyr和Arg侧链作为氢键供体参与的证据。
7. Study on the Preparation of Biohydrocarbon Fuel by Catalytic Hydrogenation of Swida wilsoniana Pyrolysis Products [O] . Aihua Zhang, Juan Tang, Jilie Lie, 2020

机译：Swida Wilsoniana热解产物催化氢化制备生物氢碳燃料的研究
8. Experimental Study of Catalytic Hydrogenation by Using an in-Situ Hydrogen Measuring Technique. Final Report [R] . Chiang, S. H., Klinzing, G. E., Cheng, Y. S. 1984

机译：原位氢测定催化加氢实验研究。总结报告

Experimental Studies of Catalytic Hydrogenation of Isophthalonitrile for Meta-Xylenediamine Preparation

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