Synthesis and Characterization of PolyVBTMAAla

机译：聚VBTMA ALA的合成与表征

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Polymerized ionic liquids (PILs) were successfully prepared by using 4-(vinylbenzyltrimethyl)ammonium, [VBTMA] as the cation and alanine as the anion. The monomer [VBTMA]Ala was reacted with AIBN as radical initiator to produce poly[VBTMA]Ala. The polymer was characterized by using NMR and FTIR. Thermal degradation behavior for Poly[VBTMA]Ala was 168.70 °C and glass transition temperature (T_g) was not detected even at second cycle. The surface area, pore size and pore volume were determined by using BET surface area and pore size analyzer which showed that Poly[VBTMA]Ala has mesoporous structure. The morphology was determined by FESEM. The CO_2 adsorption was measured by gas adsorption cell which showed that the mole of CO_2 adsorb increased as pressure increased.

机译：通过使用4-（乙烯基苄基三甲基）铵，[VBTMA]作为阴离子，成功制备聚合离子液体（PILs）。单体[VBTMA] ALA与AIBN作为自由基引发剂反应以产生聚[VBTMA] ALA。使用NMR和FTIR的特征在于该聚合物。甚至在第二循环中，均匀未检测到聚[VBTMA] ALA的热降解行为为168.70℃，玻璃化转变温度（T_G）。通过使用BET表面积和孔径分析仪测定表面积，孔径和孔体积，所述孔径分析仪显示POLY [VBTMA] ALA具有中孔结构。通过FeSem确定了形态。通过气体吸附细胞测量CO_2吸附，所述气体吸附细胞显示，随着压力增加，CO_2吸附摩尔的摩尔摩尔摩尔含量增加。

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《International Conference on Fundamental and Applied Sciences》|2014年||共7页
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M.S. Raja Shahrom; C.D. Wilfred; F.K. Chong;
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中图分类 TB11-532;
关键词
cation; anion; monomer;

机译：阳离子;阴离子;单体;

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Synthesis and Characterization of PolyVBTMAAla

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