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Analytical validation applied to simultaneous determination of solvents dichloromethane (DCM), methyl isobutyl ketone (MIBK), tetrahydrofuran (THF) and toluene (TOL) in urine by headspace extraction and injection on chromatographic system with a flame io nization detector

机译：通过具有火焰IO nization检测器的色谱系统，尿液中尿液中溶剂二氯甲烷（DCM），甲基异丁基酮（MIBK），四氢呋喃（THF），四氢呋喃（THF）和甲苯（TH1）的分析验证

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The determination of the volatile organic solvents dichloromethane (DCM), methyl isobutyl ketone (MIBK), tetrahydrofuran (THF) and toluene (TOL) is applied on toxicological monitoring of employees in various industrial activities. The gas chromatography technique with flame ionization detector and headspace injection system has been applied. The analytical procedure developed allows the simultaneous determination of the above-mentioned solvents and the accuracy of the method was tested following the INMETRO guidelines through the DOQ-CGRE 008 Rev.04-July/2011.

机译：挥发性有机溶剂二氯甲烷（DCM），甲基异丁基酮（MIBK），四氢呋喃（THF）和甲苯（TOL）的测定适用于各种工业活动中员工的毒理学监测。采用了具有火焰电离检测器和顶空注射系统的气相色谱技术。开发的分析程序允许同时测定上述溶剂，并通过Doq-CGRE 008-juls / 2011的Inmedro指南测试方法的准确性。

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《Brazilian Congress on Metrology》|2015年|544p|共6页
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E D M Muna; R P Pereira;
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1. H-ZSM-5分子筛在H2O−四氢呋喃/2-丁醇/2-甲基四氢呋喃反应体系中催化葡萄糖转化制备5-羟甲基糠醛 [J] . 徐思泉, 潘东辉, 肖国民中南大学学报（英文版） . 2019,第011期
2. Analytical validation applied to simultaneous determination of solvents dichloromethane (DCM), methyl isobutyl ketone (MIBK), tetrahydrofuran (THF) and toluene (TOL) in urine by headspace extraction and injection on chromatographic system with a flame ionization detector [J] . E D M Muna, R P Pereira Journal of Physics: Conference Series . 2016,第1期

机译：分析验证适用于通过顶空萃取并在色谱系统上通过火焰离子化检测器进样同时测定尿中的溶剂二氯甲烷（DCM），甲基异丁基酮（MIBK），四氢呋喃（THF）和甲苯（TOL）
3. Determination of methyl ethyl ketone in urine samples by headspace solid phase micro extraction (SPME) sampling associated to gas chromatography with flame-ionization detectoR (GC-FID) [J] . Antunes Marina Venzon, Centro Universitário Feevale Rodovia Novo Hamburgo Brasil, Linden Rafael Quimica nova . 2008,第8期

机译：顶空固相微萃取（SPME）采样与火焰离子化气相色谱（GC-FID）气相色谱法一起测定尿液样品中的甲乙酮
4. Analytical validation applied to simultaneous determination of solvents dichloromethane (DCM), methyl isobutyl ketone (MIBK), tetrahydrofuran (THF) and toluene (TOL) in urine by headspace extraction and injection on chromatographic system with a flame io nization detector [C] . E D M Muna, R P Pereira Brazilian Congress on Metrology . 2015

机译：通过具有火焰IO nization检测器的色谱系统，尿液中尿液中溶剂二氯甲烷（DCM），甲基异丁基酮（MIBK），四氢呋喃（THF），四氢呋喃（THF）和甲苯（TH1）的分析验证
5. Determinação de metil-etil-cetona em amostras de urina com amostragem por micro extração em fase sólida (MEFS) em headspace associada à cromatografia gasosa com detector de ionização de chama (CG-DIC) Determination of methyl ethyl ketone in urine samples by headspace solid phase micro extraction (SPME) sampling associated to gas chromatography with flame-ionization detectoR (GC-FID) [O] . Marina Venzon Antunes, Rafael Linden 2008

机译：固相微萃取（MEFS）顶空进样与火焰色谱电离检测器（CG-DIC）气相色谱法一起测定尿样中的甲基乙基酮顶空固体测定尿样中的甲基乙基酮气相色谱与火焰电离检测器（GC-FID）关联的气相微萃取（SPME）采样

Analytical validation applied to simultaneous determination of solvents dichloromethane (DCM), methyl isobutyl ketone (MIBK), tetrahydrofuran (THF) and toluene (TOL) in urine by headspace extraction and injection on chromatographic system with a flame io nization detector

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