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Microstructure/Properties Relationship of Advanced Heat-Resistant Intermetallics TiAl(Nb,Cr,Zr) After Casting and Float Zone Processing

机译:高级耐热物质金属间(NB,CR,Zr)铸造浮区加工的微观结构/性能关系

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New Ti-44Al-5Nb-3Cr-1.5Zr (at.%) β-stabilized intermetallic alloy was synthesized by the electron beam casting and afterwards re-solidified by the high-gradient (300 °C cm~(-1)) induction float zone (FZ) technique. FZ-processing led to the ordered microstructure creation consisting of volumetrically prevailing (γ + α_2) lamellar colonies separated by minor seam-like γ-granular interlayers, and the least intergranular quota of β(Ti)/B2 phase. The optimum phase balance, submicron interlamellar spacing and preferable alignment of lamellae along the thermal gradient were controlled by FZ-conditions. Unique microstructural adjustment enhances drastically the high-temperature yield strength, Young modulus and creep resistance. Thus the thermal limit of γ-TiAl(Nb,Cr,Zr) structural applicability could be extended from 750–800 °C towards 900–950 °C.
机译:通过电子束铸件合成新的Ti-44AL-5NB-3CR-1.5ZR(AT.%)β-稳定的金属间合金。之后通过高梯度(300℃Cm〜(-1))诱导重新固化浮区(FZ)技术。 FZ处理导致由由小接缝γ-粒状中间层分离的体积普遍(γ+α_2)层状组成的有序的微观结构,以及β(Ti)/ B2相的最小晶间配额。通过FZ条件控制沿着热梯度的最佳相平衡,亚微米层间距和Lamellae的优选对准。独特的微观结构调节急剧增强了高温屈服强度,幼年模量和蠕变性。因此,γ-Tial(Nb,Cr,Zr)结构适用性的热限率可以延伸到900-950℃。

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