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Preparation of Activated Carbon and Zeolite NaA Composites from Rice Husk charcoal for Water Filtration

机译:从稻壳炭的制备液体过滤中的稻壳炭炭和沸石Naa复合材料

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Carbon and amorphous silica from rice husk charcoal was prepared by carbonization of rice husk in an incineration furnace around 700°C. The rice husk charcoal was taken as a precursor in the synthesis of carbon and zeolite NaA composites by hydrothermal method at various synthesis temperatures of 80-110°C and for 2-8 hour. The composite powder was formed into rectangular shape of 10 mm width, 60 mm length and 10 mm thickness by hydraulic pressing at 60 MPa with 1% of carboxy methyl cellulose mixed with 5-20% of phenolic resin as binders. Samples were fired in a tubular furnace with 5% CO_2+N_2 gas flow at 300-700°C for 1 hour as the thermal activation of carbon and sintering of the composite samples. Activated carbon and zeolite NaA composites were characterized in terms of phase analysis, morphology, thermal stability, mechanical strength, calcium ions absorbtivity and specific surface area by x-ray diffraction (XRD), scanning electron microscopy (SEM), thermogravimetric analysis (TGA), three points bending, inductive coupled plasma-optical emission spectroscopy (ICP-OES) and brunauer-emmett-teller technique (BET), respectively.
机译:通过在焚烧炉中碳化在700℃下的焚烧炉中碳化制备来自水稻壳木炭的碳和无定形二氧化硅。在各种合成温度为80-110℃和2-8小时的水热法,将稻壳木炭作为合成碳和沸石NAA复合材料的前体。通过在60MPa的60MPa下用液压压制,将复合粉末形成10mm宽度,60mm长度和10mm厚的矩形,其中1%的羧基甲基纤维素与5-20%的酚醛树脂作为粘合剂混合。将样品在管状炉中用5%CO_2 + N_2气流烧成300-700℃的1小时作为复合样品的碳和烧结的热活化。通过X射线衍射(XRD),扫描电子显微镜(SEM),热重分析(TGA),在相位分析,形态,热稳定性,机械强度,钙离子吸收和比表面积,扫描电子显微镜(SEM),热重分析(TGA)方面,表征活性炭和沸石NAA复合材料。 ,三个点弯曲,电感耦合等离子体光发射光谱(ICP-OES)和Brunauer-Emmett-Teller技术(BET)。

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