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Preparation of Zirconium Diboride Nano-Powders Using Different Zirconium Sources via Sol-Gel Method

机译:用溶胶 - 凝胶法制备不同锆源的锆二硼化锆纳米粉末

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Zirconium diboride nano-powders were synthesized by sol-gel method using different zirconium sources of zirconium carbonate and zirconium nitrate based on different gelling processing. Both of zirconium source can be applied in the synthesis of good performance ZrB_2 powders while the in-suit sol-gel using zirconium carbonate tend to form the spherical ZrB_2 powders about 50nm and the sol-gel using zirconium nitrate prefer to form worm ZrB_2 powders about 200nm. The influences of B/Zr molar ration of zirconium carbonate and zirconium nitrate of sol-gel method on the phase constitution was investigated. And the gel mechanism was discussed to explain the different phase constitution, morphology of final products.
机译:使用不同的锆碳酸锆和硝酸锆基于不同的胶凝加工,通过溶胶 - 凝胶法合成氧化锆纳米粉末。锆源都可以应用于良好的性能ZrB_2粉末的合成,同时使用锆碳酸锆的加入式溶胶 - 凝胶倾向于形成约50nm的球形ZrB_2粉末,并使用硝酸锆优选形成蠕虫Zrb_2粉末的溶胶 - 凝胶。 200nm。研究了B / ZR摩尔锂摩尔醇酸盐和硝酸锆硝酸锆法对相体构成的影响。讨论了凝胶机制以解释不同的相体系,最终产品的形态。

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