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Optical Properties of Fe3O4 Thin Films Prepared from the Iron Sand by Spin Coating Method

机译:Fe3O4薄膜的光学性质通过旋涂法制备铁砂制备

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Research on magnetic oxide is growing very rapidly. This magnetic oxide can be found in nature that is in iron sand. One of the beaches in Sumatera Barat containing iron sand is Tiram Beach, Padang Pariaman District, Sumatera Barat. The content of iron sand is generally in the form of magnetic minerals such as magnetite, hematite, and maghemit-Magnetite has superior properties that can be developed into thin films. The purpose of this research is to investigate the optical properties of transmittance, absorbance, reflectance and energy gap from Fe3O4 thin films. This type of research is an experimental research. The iron sand obtained from nature is first purified using a permanent magnet, then made in nanoparticle size using HEM-E3D with milling time for 30 hours. After that, the process of making thin film with sol-gel spin coating method. In this research, variation of rotation speed from spin coating is 1000 rpm, 2000 rpm and 3000 rpm. Based on XRD results indicated that the iron sand of Tiram beach contains magnetite minerals and the SEM results show that the thickness of the thin films formed is 25μm, 24μm and Hum. The characterization tool used for characterizing optical properties is the UV-VIS Spectrophotometer. So it can be concluded that the greater the speed of rotation the thickness of the thin layer will be smaller, resulting in the transmittance and reflectance will be greater, while the absorbance will be smaller. Energy gap obtained from this research is 3,75eV, 3,75eV and 3,74eV. So the average energy gap obtained is 3,75eV.
机译:磁氧化物的研究非常迅速增长。这种磁性氧化物可以在铁砂中找到。桑拉特铁沙萨拉特的海滩之一是泰兰海滩,巴东巴塔岛巴塔岛地图港市区区。铁砂的含量通常是磁性矿物质的形式,例如磁铁矿,赤铁矿,磁石 - 磁铁矿具有优异的性能,可以发展成薄膜。本研究的目的是研究来自Fe3O4薄膜的透射率,吸光度,反射率和能隙的光学性质。这种研究是一个实验研究。首先使用永磁体纯化自制性的铁砂,然后在纳米颗粒尺寸下使用磨削时间进行30小时。之后,用溶胶 - 凝胶旋涂法制备薄膜的方法。在本研究中,旋转涂层的转速变化为1000rpm,2000rpm和3000rpm。基于XRD结果表明,蒂拉姆海滩的铁砂含有磁铁矿矿物质,SEM结果表明,形成的薄膜的厚度为25μm,24μm和嗡嗡声。用于表征光学性质的表征工具是UV-Vis分光光度计。所以可以得出结论,薄层厚度越大的旋转速度越大,导致透射率和反射率将会更大,而吸光度将更小。从本研究获得的能隙为3,75EV,3,75EV和3,74EV。所以获得的平均能量差距为3,75EV。

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