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Optimization of palm oil extraction from Decanter cake of small crude palm oil mill by aqueous surfactant solution using RSM

机译:用RSM含水表面活性剂溶液中小原油棕榈油磨削岩油萃取棕榈油萃取优化

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The use of hexane to extract vegetable oil from oilseeds or seed cake is of growing concern due to its environmental impact such as its smelling and toxicity. In our method, used Response Surface Methodology (RSM) was applied to study the optimum condition of decanter cake obtained from small crude palm oil with aqueous surfactant solution. For the first time, we provide an optimum condition of preliminary study with decanter cake extraction to obtain the maximum of oil yield. The result from preliminary was further used in RSM study by using Central Composite Design (CCD) that consisted of thirty experiments. The effect of four independent variables: the concentration of Sodium Dodecyl Sulfate (SDS) as surfactant, temperature, the ratio by weight to volume of cake to surfactant solution and the amount of sodium chloride (NaCl) on dependent variables are studied. Data were analyzed using Design-Expert 8 software. The results showed that the optimum condition of decanter cake extraction were 0.016M of SDS solution concentration, 73°C of extraction temperature, 1:10 (g:ml) of the ratio of decanter cake to SDS solution and 2% (w/w) of NaCl amount. This condition gave 77.05% (w/w) oil yield. The chemical properties of the extracted palm oil from this aqueous surfactant extraction are further investigated compared with the hexane extraction. The obtained result showed that all properties of both extractions were nearly the same.
机译:使用己烷从油籽或种子蛋糕中提取植物油由于其环境影响而产生的令人担忧,例如其嗅觉和毒性。在我们的方法中,应用了使用的响应表面方法(RSM)来研究从具有水性表面活性剂溶液的小粗棕榈油获得的滗析饼的最佳条件。我们首次提供了用滗析器蛋糕提取的初步研究的最佳条件,以获得油产量的最大值。通过使用第三种实验组成的中央复合设计(CCD),初步的结果进一步用于RSM研究。四种独立变量的影响:研究了十二烷基硫酸钠(SDS)作为表面活性剂,温度,对表面活性剂溶液的重量比的重量比与氯化钠(NaCl)的浓度为依赖性变量。使用设计专家8软件分析数据。结果表明,滗蚀剂萃取的最佳条件为0.016m的SDS溶液浓度,73℃的提取温度,1:10(g:ml)滗析器滤饼与SDS溶液的比例和2%(w / w )NaCl量。该条件给出了77.05%(w / w)油产率。与己烷萃取相比,进一步研究了来自该水性表面活性剂萃取的提取的棕榈油的化学性质。得到的结果表明,两种萃取的所有性质几乎是相同的。

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