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Effect of the Mechanical Alloying and Spark Plasma Sintering on Microstructure, Phase Composition and Chemical Elements Distribution of Nb-Si Based Composite

机译:机械合金化和火花等离子体烧结对Nb-Si基复合材料的微观结构,相组合物和化学元素分布的影响

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Synthesis of the Nb-Si in-situ composite was attempted by mechanical alloying of element powders in vario-planetary ball mill. The particles size distribution was measured by laser diffraction, microstructures were examined with scanning electronic microscope, and the phase constituent were analyzed by X-ray diffraction. The amorphization of the Si during mechanical alloying, large amount of deformation of Nb crystal structure, and after all - the formation of supersaturated solid solution of Nb was observed. To stabilize microstructure and phase composition, a spark plasma sintering was attempted. After SPS microstructure consist of three main phases - Nb_(ss), Nb_5Si_3 and Nb_3Si.
机译:通过机械合金化元件粉末在变型行星球磨机中的机械合金,试图合成Nb-Si原位复合材料。通过激光衍射测量颗粒尺寸分布,用扫描电子显微镜检查微观结构,通过X射线衍射分析相位成分。在机械合金化期间Si的大杂化,Nb晶体结构的大量变形以及之后 - 观察到Nb的超饱和固溶体的形成。为了稳定微观结构和相组合物,尝试了火花血浆烧结。 SPS微结构组成三个主要阶段 - NB_(SS),NB_5SI_3和NB_3SI之后。

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