• 主题
高级搜索  >
历史搜索 清空历史
首页> 外文会议>International Conference on X-Rays and Related Techniques in Research and Industry >Synthesis of 4-methyl-N-(2-pyridine-2-yl-ethyl)carbamothioylbenzamide-Si02 Hybrid Mesoporous Material from Rice Husk
【24h】

Synthesis of 4-methyl-N-(2-pyridine-2-yl-ethyl)carbamothioylbenzamide-Si02 Hybrid Mesoporous Material from Rice Husk

机译：4-甲基-N - （2-吡啶-2-基乙基）氨基甲酰-SI02杂交中孔材料的合成稻壳

获取原文
页面导航
  • 摘要
  • 著录项
  • 相似文献
  • 相关主题

摘要

4-methyl-N-[(2-pyridine-2-yl-ethyl)carbamothioyl]benzamide (P2) was synthesized and covalently bonded to silica. This new heterogeneous catalyst was labelled as RHACP2. The SEM image of this hybrid thiourea silicate can be seen as aggregate particles. The surface morphology revealed spherical and irregular nanoparticles. The SEM images shows mesoporous solids containing agglomerates of spherical particles of fairly uniform size and array. The TEM images with irregular shape of porosity could be clearly observed and in general supported the amorphous nature of RHACP2. The XRD indicates the catalyst to be amorphous. The nitrogen adsorption-desorption isotherm of the catalyst shows the mesoporous property. It shows a type-IV curve with hysteresis loop.
机译：合成4-甲基-N - [（2-吡啶-2-基乙基）氨基甲酰基甲酰胺（P2），并与二氧化硅共价键合。将该新的异构催化剂标记为rhacP2。该杂交硫脲硅酸盐的SEM图像可以被视为骨料颗粒。表面形态显示球形和不规则的纳米颗粒。 SEM图像显示含有相距的球形颗粒的介孔固体，其尺寸和阵列的球形颗粒。可以清楚地观察具有不规则形状的孔隙率形状的TEM图像，并且通常支持rhacP2的无定形性质。 XRD表示催化剂是无定形的。催化剂的氮吸附 - 解吸等温摩迹显示了中孔的性质。它显示了一种带滞后回路的IV型曲线。

著录项

相似文献

  • 外文文献
  • 中文文献
  • 专利
获取原文

客服邮箱：kefu@zhangqiaokeyan.com

京公网安备：11010802029741号 ICP备案号：京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有

  • 客服微信

  • 服务号