Optimization of Chromatographic Parameters for the Determination of Benzo(a)pyrene in Frying Oil by High-Performance Liquid Chromatography

机译：优化高效液相色谱法测定苯并（A）芘测定苯并（A）芘的色谱法

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This study was aimed to optimize the chromatographic parameters for the determination of benzo(α)pyrene in frying oil. Liquid-liquid extraction was applied to extracted benzo(α)pyrene with n-hexane and, then analysed by high-performance liquid chromatography with ultraviolet visible detection. Data analysis suggested that good separation effect could be gained when acetonitrile and water had a ratio of 88:12. Flow rate of mobile phase of l.0ml/min was settled. The column temperature was set at 30 °C based on analysis time and separation effect.

机译：本研究旨在优化用于测定盐水中苯并（α）芘的色谱参数。液 - 液萃取被施加用正己烷萃取苯并（α）芘，然后通过高性能液相色谱法与紫外线检测分析。数据分析表明，当乙腈和水的比例为88:12时，可以获得良好的分离效果。 L.0ml / min的流动相的流速稳定。基于分析时间和分离效果，在30℃下设定柱温。

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《International Forum on Materials Science and Industrial Technology》|2013年||共4页
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作者
Bin Deng;
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原文格式 PDF
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中图分类 TB3-532;
关键词
Optimization; HPLC; Benzo(a)pyrene; Frying oil;

机译：优化;HPLC;苯并（A）芘;煎炸油;

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2. Determination of benzo[a] pyrene in smoked foods by high-performance liquid chromatography based on magnetic solid phase extraction [J] . Pan Yan, Deng Zhifen, Chen Yanlong, Analytical methods . 2017,第39期

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机译：用荧光检测快速测定高效液相色谱法测定蒽和苯并（A）芘
4. Optimization of Chromatographic Parameters for the Determination of Benzo(a)pyrene in Frying Oil by High-Performance Liquid Chromatography [C] . Bin Deng International Forum on Materials Science and Industrial Technology . 2013

机译：优化高效液相色谱法测定苯并（A）芘测定苯并（A）芘的色谱法
5. Chromatographic, spectroscopic, and electrochemical studies of benzo(a)pyrene derivatives: 9,10 dihydrobenzo(a)pyren-7(8H)-one and 7,8,9,10-tetrahydrobenzo(a)pyrene. [D] . Sanchez, Alexis Wilfredo. 2015

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6. Determination of Aflatoxin B1 and B2 in Vegetable Oils Using Fe3O4/rGO Magnetic Solid Phase Extraction Coupled with High-Performance Liquid Chromatography Fluorescence with Post-Column Photochemical Derivatization [O] . Li Yu, Fei Ma, Liangxiao Zhang, 2019

机译：Fe3O4 / rGO磁性固相萃取-高效液相色谱-柱后光化学衍生-荧光法测定植物油中的黄曲霉毒素B1和B2
7. Optimization of High-Performance Liquid Chromatographic Parameters for the Determination of Capsaicinoid Compounds Using the Simplex Method [O] . Rachaneewan KARNKA, Mongkon RAYANAKORN, Surasak WATANESK, 2002

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8. Liquid Chromatographic Determination of Benzo(A)Pyrene at Part-Per-Billion Concentrations in Highly-Refined Coal- and Petroleum-Derived Fuels [R] . Tomkins, B. A., Griest, W. H. 1986

机译：液相色谱法测定高度精炼煤和石油衍生燃料中十分之一浓度的苯并（a）芘

Optimization of Chromatographic Parameters for the Determination of Benzo(a)pyrene in Frying Oil by High-Performance Liquid Chromatography

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