X-ray diffraction and extended X-ray absorption fine structure study using synchrotron radiation of cobalt (II) complexes

机译：X射线衍射和延长的X射线吸收细结构研究使用钴（II）复合物的同步辐射辐射

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XRD and EXAFS investigation of cobalt (II) macro cyclic complexes were carried out. These complexes were synthesised by chemical rout method. On the analysis of the complexes with X-ray diffraction (XRD) and extended X-ray absorption fine structure (EXAFS), XRD analysis shows that complexes are crystalline in nature and having particle size and lattice parameter in the rang of few micro meter and EXAFS technique extract the local structure of complexes. The nearest neighbouring atom distance commonly known as 'bond length' were calculated using Fourier transform method. The bond lengths determined from these methods were also compared with the bond length obtained from several other known technique.

机译：XRD和EXAFS对钴（II）宏观循环复合物进行的研究。通过化学溃败方法合成这些配合物。在分析X射线衍射（XRD）和延伸X射线吸收细结构（EXAFS）的分析中，XRD分析表明，复合物在自然界中是结晶，并且在少数微米的范围内具有粒度和晶格参数EXAFS技术提取复合物的局部结构。使用傅立叶变换方法计算通常称为“键合长度”的最近相邻的原子距离。还将这些方法确定的键合长度与从几种其他已知技术获得的键合长度进行比较。

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《International Conference on Recent Trends in Physics》|2014年||共4页
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Ashotosh Mishra; Kritika Shukla; Jagrati Dwivedi; Samrath Ninama;
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中图分类 O4-532;
关键词
XRD; EXAFS; having particle;

机译：XRD;外爆;有粒子;

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2. X-RAY DIFFRACTION AND EXTENDED X-RAY ABSORPTION FINE STRUCTURE (EXAFS) STUDIES OF COPPER (II) COMPLEXES WITH LIGANDS 2-METHYL-3-[(BIS-ANILINE(R) PHENYL]-3H-1, 5 BENZODIAZEPINE USING SYNCHROTRON RADIATION SOURCE [J] . AUSHTOSH MISHRA, SAMRATH NINAMA The African Physical Review . 2013,第2013期

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4. X-ray diffraction and extended X-ray absorption fine structure study using synchrotron radiation of cobalt (II) complexes [C] . Ashotosh Mishra, Kritika Shukla, Jagrati Dwivedi, International Conference on Recent Trends in Physics . 2014

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机译：使用X射线衍射和延伸X射线吸收细结构（XRD和EXAFS）苯嘧啶衍生自苯并-2,4-二硝基苯基腙的贫苯碱铜（II）复合物的表征

X-ray diffraction and extended X-ray absorption fine structure study using synchrotron radiation of cobalt (II) complexes

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