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Studies on the preparation, structure and spectral character of Yb~(3+), Er~(3+):YAG nanocrystal powders by sol-gel method

机译:用溶胶 - 凝胶法的YB〜(3+),ER〜(3 +):YAG纳米晶体粉体的制备,结构和光谱特性研究

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The Yb~(3+)-Er~(3+) co-doped YAG nanocrystal powders have been successfully prepared by the simple sol-gel method at a low temperature. The gel was prepared from nitrates of yttrium, aluminum, ytterbium, erbium and citric acid, and was heat-treated at temperatures from 800 to 1000°C. The phase purity and microstructural features of the materials were analyzed by means of X-ray diffraction (XRD) and transmission electron microscopy (TEM). TEM result shows that the YAG nanocrystal particle size is about 20-50nm. The luminescence spectra for different Yb~(3+) and Er~(3+) dopant concentration was obtained at about 1.52um which is in the eyesafe regime where significantly higher pulse energies can be used without damaging human eyes.
机译:Yb〜(3 +) - ER〜(3+)共掺杂的YAG纳米晶体粉末已通过在低温下通过简单的溶胶 - 凝胶法成功制备。 凝胶由硝酸钇,铝,镱,铒和柠檬酸制备,并在800至1000℃的温度下进行热处理。 通过X射线衍射(XRD)和透射电子显微镜(TEM)分析材料的相纯度和微观结构特征。 TEM结果表明,YAG纳米晶体粒径为约20-50nm。 在大约1.52um处获得不同Yb〜(3+)和ER〜(3+)掺杂剂浓度的发光光谱,其在眼睛内的状态下,可以使用显着更高的脉冲能量而不会损坏人眼。

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