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Obtaining of the Ir-Al Nanocrystalline Powders by Mechanical Alloying

机译:机械合金化制备Ir-Al纳米晶粉

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摘要

The Ir-AI powder in the 1:1 atomic ratio was obtained by high energy mechanical alloying in a Pulverisette 4 Fritch planetary mill. The final product was obtained after 28 h of milling in argon atmosphere. Alloy formation was investigated by X-ray diffraction. After 4 h of milling the new structure of IrAl compound is found in the diffraction patterns. The obtained powders are nanocrystalline with a mean crystallite size of 11 nm after 28 h of milling. The particle morphology and the chemical homogeneity were studied using scanning electron microscopy (SEM) and energy dispersive spectrometry (EDX). It was found that the obtained compound present large particles composed by smaller one.
机译:原子比为1:1的Ir-Al粉末是通过在Pulverisette 4 Fritch行星磨中通过高能机械合金化获得的。在氩气中研磨28小时后,获得最终产品。通过X射线衍射研究了合金的形成。研磨4小时后,在衍射图中发现了IrAl化合物的新结构。研磨28小时后,所得粉末为纳米晶体,平均微晶尺寸为11 nm。使用扫描电子显微镜(SEM)和能量色散谱(EDX)研究了颗粒的形态和化学均匀性。发现所获得的化合物存在由较小的颗粒组成的大颗粒。

著录项

  • 来源
    《Researches in Powder Metallurgy》|2009年|p.171-174|共4页
  • 会议地点 Craiova(RO);Craiova(RO)
  • 作者单位

    Materials Sciences and Technology Dept., Technical University of Cluj-Napoca, 103-105 Muncii ave., 400641 Cluj-Napoca, Romania;

    Department of Nuclear Materials, Institute for Nuclear Research, 1Campului street, 115400,Mioveni-Arges, Romania;

    Materials Sciences and Technology Dept., Technical University of Cluj-Napoca, 103-105 Muncii ave., 400641 Cluj-Napoca, Romania;

    Materials Sciences and Technology Dept., Technical University of Cluj-Napoca, 103-105 Muncii ave., 400641 Cluj-Napoca, Romania;

    Materials Sciences and Technology Dept., Technical University of Cluj-Napoca, 103-105 Muncii ave., 400641 Cluj-Napoca, Romania;

  • 会议组织
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 粉末冶金(金属陶瓷工艺);
  • 关键词

    nanocrystalline; radiation target; mechanical alloying;

    机译:纳米晶辐射目标机械合金化;

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