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Analysis of Stacking Structure of Cup-Stacked Type Carbon Nanofibers

机译:杯叠式碳纳米纤维的叠层结构分析

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摘要

The lattice images of the new type (cup-stacked type) carbon nanofibers were observed by high resolution transmission electron microscopy (HRTEM) and the detailed structure was analyzed by image processing. The angle of opposed graphitic basal planes was measured from power spectrum obtained by 2 dimensional first Fourier transform. The structures of the slanted (00 ·1) lattice planes, which appear at the cross section of the fiber wall, were shown by means of this image analysis technique. Defects were observed in the ordered structure of this material. The (00·1) lattice planes show large fluctuation in alignment of them and the (10·0) lattice planes make several angles with the (00·1) lattice planes. The average repeat distance d_(002) was estimated on the basis of d_(100) by HRTEM image and image analysis.
机译:通过高分辨率透射电子显微镜(HRTEM)观察了新型(杯叠式)碳纳米纤维的晶格图像,并通过图像处理分析了其详细结构。从通过二维第一傅里叶变换获得的功率谱测量相对的石墨基面的角度。借助这种图像分析技术,可以显示出出现在纤维壁横截面上的倾斜(00·1)晶格平面的结构。在该材料的有序结构中观察到缺陷。 (00·1)晶格的排列存在较大的波动,(10·0)晶格与(00·1)晶格成多个角度。通过HRTEM图像和图像分析基于d_(100)来估计平均重复距离d_(002)。

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