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Solid freeform fabrication of functional silicon nitride ceramics using laminated object manufacturing.

机译:使用叠层物体制造进行固态无定形功能氮化硅陶瓷的制造。

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摘要

A novel concept for the fabrication of functional structural ceramic components was investigated using rapid prototyping technology. The technology used was based on the Laminated Object Manufacturing (LOM) process for creating solid prototypes by sequentially laminating and cutting constituent cross-section layers of sheet material. In this study, the LOM process has been adapted to use green tape preforms to prepare ceramic shapes directly from Computer Aided Design (CAD) generated images.;The host material in this study, silicon nitride (Si3N 4), is an important structural ceramic due to its desirable mechanical, thermal and chemical properties. Tape preforms of Si3N4 tailored for the LOM process were fabricated using standard tape casting techniques.;Two material systems were investigated; (a) monolithic Si3 N4, and (b) a preceramic polymer infiltrated Si 3N4.;The physical and mechanical property data obtained for both monolithic and infiltrated LOM Si3N4 ceramics showed that both materials had high densities (monolithic Si3N4, average theoretical density = 97%, infiltrated Si3N4, average theoretical density = 94%) and high Young's moduli (monolithic Si3N 4 = 307 GPa, infiltrated Si3N4 = 301 GPa. Both materials also had high strengths and fracture toughnesses.;Using a preceramic polymer infiltration process reduced the inherent shrinkage that occurs during sintering of conventional ceramics. Volume shrinkage for the infiltrated LOM Si3N4 ceramics was 25% compared to 40% for the monolithic Si3N4 ceramics;The results obtained in this research demonstrated that the LOM technique is a viable method for preparing Si3N4 ceramics with good physical and mechanical properties. (Abstract shortened by UMI.)
机译:使用快速成型技术研究了一种用于制造功能性结构陶瓷组件的新颖概念。所使用的技术基于层压对象制造(LOM)工艺,该工艺通过依次层压和切割板材的组成横截面层来创建实体原型。在这项研究中,LOM工艺已被改编为使用绿色胶带预成型件直接从计算机辅助设计(CAD)生成的图像中制备陶瓷形状。;本研究的主体材料氮化硅(Si3N 4)是一种重要的结构陶瓷由于其理想的机械,热和化学特性。使用标准的流延技术制造了适合LOM工艺的Si3N4的预成形带。 (a)整体式Si3 N4,和(b)渗透到陶瓷中的Si 3N4 ;;针对整体式和渗透LOM Si3N4陶瓷的物理和机械性能数据表明,两种材料都具有高密度(整体式Si3N4,平均理论密度= 97 %,渗透的Si3N4,平均理论密度= 94%)和高的杨氏模量(整体Si3N 4 = 307 GPa,渗透的Si3N4 = 301 GPa。两种材料都具有很高的强度和断裂韧性。);使用陶瓷前体聚合物的渗透过程降低了固有的渗入的LOM Si3N4陶瓷的体积收缩率为25%,而整体式Si3N4陶瓷的体积收缩率为40%;该研究结果表明,LOM技术是一种可行的方法,用于制备具有以下特征的Si3N4陶瓷:良好的物理和机械性能(摘要由UMI缩短)。

著录项

  • 作者

    Rodrigues, Stanley John.;

  • 作者单位

    University of Dayton.;

  • 授予单位 University of Dayton.;
  • 学科 Engineering Materials Science.
  • 学位 Ph.D.
  • 年度 2000
  • 页码 155 p.
  • 总页数 155
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 人类学;
  • 关键词

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