Homochiral bis[(O,O'-di-2-isopropyl-5-methylcyclohexyl) dithiophosphato] nickel(Ⅱ) (1), prepared by the reaction of O,O'-di-2-isopropyl-5-methylcyclohexyl) dithiophosphato potassium with Ni(OAc)2 displays a almost planar tetragonal geometry around Ni center composed of four S atoms from two different ligands. CCDC: 252341.
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