An azobenzene compound with terminal diethynyl was synthesized by diazo coupling reaction, metallic padallium catalyzed reaction and Williamson method. Its structures were characterized by IR, 1H NMR and DSC.%采用偶氮偶联、金属钯催化偶联法和Williamson醚合成法,合成了一种末端双炔类偶氮化合物,其结构经IR、1H NMR、DSC分析表征.
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