Objective To study the quality standards of Alhagi sparsifolia shap. Methods The impurity limit, moisture content, total ash were determined based on the procedures records in the Appendix IX A, IX H and IX K of pharmacopoeia (published in 2010). The thin layer chromatography (TLC) method was established. The rutin was determined by HPLC (the Appendix VI D). ResμLt Impurities were no more than 0.5%, the moisture content was no more than 10% and the total ash was no more than 12%. The TLC spots were clear and specific, and the rutin showed a good linear relationship at a range of 5.05~101μg with the regression equation as Y=3.264 59×10 8X-1.537 145×10-4, r=0.999 9. RSD=233% (n=6). And the average recovery was 97.8%. Conclusion The method was easy, accurate, quick and reproducible which was benefit for the quality control of Alhagi sparsifolia shap.%目的 建立维药骆驼刺的质量标准.方法 采用《中华人民共和国药典》2010年版(一部)附录ⅨA杂质检查法、附录ⅨH烘干法和附录ⅨK总灰分测定方法检查药材的杂质、水分和总灰分,采用附录Ⅵ B薄层色谱法建立定性鉴别骆驼刺的方法；采用附录Ⅵ D高效液相色谱法测定药材中芦丁的含量.结果 骆驼刺含杂质应不得超过0.5％,水分应不得超过10％,总灰分应不得超过12％；薄层色谱斑点清晰,专属性强；芦丁在5.05-101μg范围内线性关系良好,回归方程:Y=3.26459×10-8X-1.537145 × 10-4,r=0.9999,加样回收率为97.8％,RSD=2.33％(n=6).结论 该方法简便、准确、重复性好,有助于维药骆驼刺的质量控制.
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