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A revised method for determination of dialkylphosphate levels in human urine by solid-phase extraction and liquid chromatography with tandem mass spectrometry: application to human urine samples from Japanese children

机译：固相萃取和液相色谱-串联质谱法测定人尿中磷酸二烷基酯含量的修订方法：应用于日本儿童的人尿样品

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摘要

ObjectivesBiological monitoring of organophosphorus insecticide (OP) metabolites, specifically dialkylphosphates (DAP) in urine, plays a key role in low-level exposure assessment of OP in individuals. The aims of this study are to develop a simple and sensitive method for determining four urinary DAPs using high-performance liquid chromatography with tandem mass spectrometry (LC–MS/MS), and to assess the concentration range of urinary DAP in Japanese children.

机译：目的对尿液中有机磷杀虫剂（OP）代谢产物，特别是磷酸二烷基酯（DAP）的生物监测，在个人对OP的低水平接触评估中起着关键作用。这项研究的目的是开发一种简单而灵敏的方法，使用高效液相色谱-串联质谱法（LC-MS / MS）测定四种尿中DAP，并评估日本儿童中尿DAP的浓度范围。

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期刊名称 Environmental Health and Preventive Medicine
作者
Jun Ueyama; Isao Saito; Ayuko Takaishi; Hiroshi Nomura; Mai Inoue; Aya Osaka; Yuka Sugiura; Yumi Hayashi; Shinya Wakusawa; Hiroko Ogi; Kimio Inuzuka; Michihiro Kamijima; Takaaki Kondo;
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作者单位

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年(卷),期 2014(19),6
年度 2014
页码 405–413
总页数 9
原文格式 PDF
正文语种
中图分类公共卫生工程;
关键词
Organophosphorus insecticide Dialkylphosphate Human urine sample LC–MS/MS Solid-phase extraction;

机译：有机磷杀虫剂;磷酸二烷基酯;人尿液样品;LC–MS / MS;固相萃取;

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专利

1. A revised method for determination of dialkylphosphate levels in human urine by solid-phase extraction and liquid chromatography with tandem mass spectrometry: application to human urine samples from Japanese children [J] . Jun Ueyama, Isao Saito, Ayuko Takaishi, Environmental health and preventive medicine . 2014,第6期

机译：固相萃取和液相色谱-串联质谱法测定人尿中磷酸二烷基酯含量的修订方法：应用于日本儿童的人尿样品
2. Solid-phase extraction and liquid chromatography/tandem mass spectrometry assay for the determination of pitavastatin in human plasma and urine for application to Phase I clinical pharmacokinetic studies [J] . Di B, Su MX, Yu F, Journal of chromatography, B. Analytical technologies in the biomedical and life sciences . 2008,第1a2期

机译：固相萃取和液相色谱/串联质谱测定法测定人血浆和尿液中匹伐他汀的含量，用于一期临床药代动力学研究
3. Development of a method of hollow fiber-based solid-phase microextraction followed by ultra performance liquid chromatography-tandem mass spectrometry for determination of five antipsychotics in human whole blood and urine [J] . Journal of chromatography, A: Including electrophoresis and other separation methods . 2020,第期

机译：开发中空纤维的固相微萃取方法，然后进行超级性能液相色谱 - 串联质谱法测定人类全血和尿液中的五种抗精神病药
4. Gas-chromatography-tandem mass spectrometry (GC-MS) method for the determination of glycerol in human urine samples [C] . Manuela Dobrescu, Mirela Zorio, Mihai Ionica Advanced Topics in Optoelectronics, Microelectronics, and Nanotechnologies . 2019

机译：气相色谱 - 串联质谱（GC-MS）用于测定人尿液中甘油的方法
5. I. Development of a passive sampler and static sampling chamber to measure personal exposure to gaseous PAHs. II. Method development for determination of current-use and persistent pesticides in cow milk, human breast milk, baby formulas, and human serum using gas chromatography tandem mass spectrometry. [D] . Chen, Xianyu. 2012

机译：I.开发无源采样器和静态采样室以测量个人对气态多环芳烃的暴露。二。气相色谱串联质谱法测定牛奶，人母乳，婴儿配方食品和人血清中的当前和持久性农药的方法开发。
6. A novel validated procedure for the determination of nicotine eight nicotine metabolites and two minor tobacco alkaloids in human plasma or urine by solid-phase extraction coupled with liquid chromatography-electrospray ionization-tandem mass spectrometry [O] . Eleanor I Miller, Hye-Ryun K Norris, Douglas E Rollins, -1

机译：对于尼古丁的确定一种新的验证过程八种尼古丁代谢物和耦合用液相色谱 - 电喷雾串联质谱在人血浆或尿两个次要烟草生物碱通过固相萃取
7. A revised method for determination of dialkylphosphate levels in human urine by solid-phase extraction and liquid chromatography with tandem mass spectrometry: application to human urine samples from Japanese children [O] . Jun Ueyama, Isao Saito, Ayuko Takaishi, 2014

机译：通过固相萃取和液相色谱法测定人尿液中二烷基磷酸水平的修订方法，串联质谱：施用对日本儿童的人类尿液样本

A revised method for determination of dialkylphosphate levels in human urine by solid-phase extraction and liquid chromatography with tandem mass spectrometry: application to human urine samples from Japanese children

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