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Characterization Study of Empty Fruit Bunch (EFB) Fibers Reinforcement in Poly(Butylene) Succinate (PBS)/Starch/Glycerol Composite Sheet

机译:聚(丁烯)琥珀酸盐(PBS)/淀粉/甘油复合片材中空果束(EFB)纤维增强物的特征研究

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摘要

In this study, a mixture of thermoplastic polybutylene succinate (PBS), tapioca starch, glycerol and empty fruit bunch fiber was prepared by a melt compounding method using an industrial extruder. Generally, insertion of starch/glycerol has provided better strength performance, but worse thermal and water uptake to all specimens. The effect of fiber loading on mechanical, morphological, thermal and physical properties was studied in focus. Low interfacial bonding between fiber and matrix revealed a poor mechanical performance. However, higher fiber loadings have improved the strength values. This is because fibers regulate good load transfer mechanisms, as confirmed from SEM micrographs. Tensile and flexural strengths have increased 6.0% and 12.2%, respectively, for 20 wt% empty fruit bunch (EFB) fiber reinforcements. There was a slightly higher mass loss for early stage thermal decomposition, whereas regardless of EFB contents, insignificant changes on decomposition temperature were recorded. A higher lignin constituent in the composite (for high natural fiber volume) resulted in a higher mass residue, which would turn into char at high temperature. This observation indirectly proves the dimensional integrity of the composite. However, as expected, with higher EFB fiber contents in the composite, higher values in both the moisture uptake and moisture loss analyses were found. The hydroxyl groups in the EFB absorbed water moisture through formation of hydrogen bonding.
机译:在该研究中,通过使用工业挤出机的熔体配合方法制备热塑性聚丁烯琥珀酸酯(PBS),木薯淀粉,甘油和空果束纤维的混合物。通常,插入淀粉/甘油的插入提供了更好的强度性能,但对所有标本的热量和水吸收更差。焦点研究了纤维负荷对机械,形态,热和物理性质的影响。纤维和基质之间的低界面键合显示了机械性能差。然而,更高的纤维载荷具有改善强度值。这是因为纤维调节良好的负载转移机制,如SEM显微照片所确认。拉伸和抗弯强度分别增加了6.0%和12.2%,对于20wt%的空果束(EFB)纤维增强剂。早期热分解具有略高的质量损失,而无论EFB内容物如何,记录了对分解温度的微不足道的变化。复合材料(用于高天然纤维体积)的更高的木质素成分导致较高的质量残余物,其将在高温下变成焦炭。该观察间接证明了复合材料的尺寸完整性。然而,如预期的那样,在复合材料中具有更高的EFB纤维含量,发现含水量吸收和水分损失分析的较高值。 EFB中的羟基通过形成氢键吸收水分。

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